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The research was performed by isolating some species of soil- fungi from agricultural soils handling with different pesticides and fungicides. Where the following fungi were isolated: Aspergillus niger (The isolates A1 and A2), Fusarium oxysporum ( The isolate F), Trichoderma harzianum (The isolate T). Also F. solani (The isolate F7) and T. viride (The isolate T.v) were used, whereas they were taken from high studies laboratory- Science Faculty- Tishreen University at a previous search. The research was conducted to assay the ability of the previous fungi to degradation a number of pesticides, the insecticide "Dolan", the insecticide "Plantocide", the nematicide "Vydate" and the fungicide "Bayfidan", through the effect of double dose of each pesticides in the biomass of the studied fungi on PDB medium. In addition to analysis the results residues of pesticides using Spectrophotometer, and evaluation the pH values.
This study was carried out to determine the total content of flavonoids of dried and fresh hawthorn flowers and leaves in water and hydroalcolic extracts. The method of cold and hot maceration was used to prepare these extracts. The active compound s which were found in these extracts were detected by many chemical reactions. The results of these tests showed that the extracts contain: phenols, flavonoids, and saponins.The total content of flavonoids was determined using spectrophotometric methods by forming complex with aluminum chloride and measurement absorbance at 510nm, it has been shown that quantity of flavonoids in dried samples ranges from 0.16 to 1%, while it's quantity in fresh samples 0.026- 0.18%.
Benzoic acid is extensively used in the preservation of food products for maintaining quality and extending shelf life by inhibiting mould and bacteria growth. Some previous studies have demonstrated that consumption of excessive amounts of benzoi c acid could be a health hazard. The aim of this study was to detect the presence of benzoic acid and its salts in some commercial children food like potatochips that labeled "Free of Preservatives" . Twenty seven samples of potatochips purchased from three different local products were analyzed for the presence of benzoic acid. The results revealed the presence of benzoic acid in nine samples and its concentration was between 100.34-188.65mg/kg. We have concluded also that TLC is a very convenient method for the detection of benzoic acid in food products .
The aim of this study was evaluation the effective of chelating solutions 17% EDTA, 0.2% Chitosan and 10% Sodium citrate by comparing the concentrations of chelated calcium ions after (1min-5min-24h) of application. The study was performed on 45 extracted single-rooted sound human. The sample was randomly divided into groups (n=3), each group 15 teeth that depend on the used solution.
The thin films of TiO2 were prepared by the Sol-Gel, on glass subtracts by using the following initial solutions: trichlorethylene titanium, ethanol, sodium hydroxide and hydrochloric acid and distilled water. The films were annealed at temperatur es(200- 300- 400-500)c° for 1 hour. The structure of the prepared and annealed films were studied by XRD. The XRD rusltes showed that the films prepared crystallize according to orthorhombic Structure.Lattice constants were calculated and it was found that it was consistent with the data JPCDS and with some scientific works.
In this research two analytical methods were developed for the determination of Azelastin as raw material and in Nasal Spray formulation. The first method was spectrophotometric while the other used the technic of HPLC The first method based on meas uring the absorbance at λmax 284 nm . The relationship between the absorbance and the concentration is rectilinear over the range 0.001 – 0.008 g %. The proposed spectrophotometric method was successfully applied to the determination of Azelastin in nasal spray. The percentage recoveries were 99.378±1 (10 duplicate readings)1 No interference was noticed from co-formulated drugs. For the absorbance at λmax the obtained results were in good agreement with which obtained by the Pharmacopeia method. The substance gave a good separation while the retention time was 1.467 min.
Breast cancer is one of the most common cancers in women; one of nine women will have breast cancer in her life time. Tamoxifen is the trans-isomer of a triphenylethylene derivative. The aim of this study is to evaluate the quality and the quantit y of the commercial brands of Tamoxifen 10 mg tablets which are registered and marketed in Yemen.
Fluoride ion is present in high concentration in some regions in Syria. As fluoride occurs naturally in water, We have studied some methods of fluoride removal such as Nalgonda technique and activated carbon method. In Nalgonda technique we add Al um and lime to the water, and we have found that fluoride removal efficiency remains constant when the initial concentrations of fluoride changes, or when the chloride ions exists in water, but it depends on pH, and get better when the method is investigated in two steps. In addition, adsorption of fluoride decreases with increasing sedimentation time, or using Ventilated lime or CaCO3 instead of Ca (OH)2. In activated carbon method we have done different experiments by using charcoal of coconut coir, date seeds and olive seeds. And we have found that olive seeds carbon is better than others, and its fluoride removal efficiency increases after impregnation with solution of 2% Al2(SO4)3.
Four different brands of black tea and one brand of green tea commonly available in Syrain markets were tested to measure the level of fluoride contained in their liquid using four different methods of infusion and utilizing the spectrophotometer technology: A. Infusion without boiling. B. Infusion with boiling. C. Repeated infusion. D. Continuous infusion. The results have indicated that the average level of fluoride in the samples of black tea liquid is higher than the one in the green tea sample regardless of the infusion method used. Also, it was found that the level of fluoride released from all samples is higher when boiling them in water from 1 to 5 minutes. In addition, it was proved that the level of fluoride in tea liquids is higher when it’s prepared using repeated infusion, but it’s lower when the tea has been prepared using the continuous infusion method. Tea brands (2) and (4) released the highest level of flouride 7.37mg/L and 5.01mg/L respectively, which are very high levels comparing to the other brands which released between 1.5mg/L to 2.7mg/L. To prevent fluoride from reaching poising levels, the total daily consumption of black tea liquid of brands (2) and (4) should not exceed 1.76L and 2.58L respectively and to avoid preparing them using the repeated and countinous infusion methods.
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