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Register a new userدراسة شروط تحضير الوسيط SBA-15-SO3H بطريقة التكاثف المشترك
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Aِl-Baath University رسالة ماجستير
Publication date
2017
fields
Chemistry
and research's language is
العربية
Created by
Shamra Editor
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يتضمن هذا البحث طريقة اصطناع وتوصيف مجموعة من الحفازات SBA-15-SO3H بطريقة التكاثف المشترك مختلفة عن بعضها بحجوم وأقطار مساماتها .
No English abstract
References used
Ryoo,R ,joo, S H , Kruk <m& Jaroniec, M (2001) Ordered Mesoporous Carbons. Adv Mater . Advanced Materials, 13(9). 677-681
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ZnCo2O4 spinel was successfully prepared via co-precipitation
process starting from corresponding metal chlorides in aqueous
solutions at pH=13. Different calcination temperatures (400-500-
600-700-800-1000oC) and different Zn:Co molar ratios (1:2
- 1:2.5) were applied in an effort to prepare this important spinel with perfect specifications starting from cheap, easy to handle inorganic precursors and using a simple process. This process was chosen for its simple requirements and the ability to modify the resulting spinel characteristics by adjusting different parameters easily like mixing temperature, time and speed and the drying conditions. The resulting samples were characterized using x-ray powder diffraction (XRPD), Fourier transform Infra-Red spectroscopy (FT-IR), Differential thermal analysis (DTA). The coloration, crystallinity size, formation and decomposition of the resulting ZnCo2O4 were found to depend on the calcination temperatures, Zn:Co molar ratio and stirring time. Results showed that ZnCo2O4 spinel was formed at relatively low temperatures. All the samples shared a cubic structure with Fd3m space group.
Zinc Chromate was synthesised by Co-precipitation
method, The synthesised samples were characterized using
X-ray powder diffraction technology (XRD).
Set temperature synthesis at 250 ℃ .
During this study, various types of silicon oxide were prepared
as aerogel and xerogel using multiple precursors and different
drying technics. Some of these samples were prepared from
Sodium silicate (waterglass) Na2SiO3 as a precursor which is a
cheap material, while others were prepared using tetraethoxysilane
(TEOS).
Our research aims to prepare ZnFe2O4 system by
CO-precipitation method in aqueous solution,starting from the
raw materials, and then studying its structure and properties .After
finishing the preparation period, we divided the precipitate in two
parts , and then we added to one of them the hydrogen peroxide and
then we dried every part alone, grind it and then we heated it at
various temperatures for two hours .
The purpose of this study was to prepare prolonged release tablets of verapamil: matrix and coated tablets, because of the importance of these systems in drug delivery and improving the patient compliance and therapeutic efficacy .Different formula
tions were prepared by using different release-modifiers polymers (EURL100 and EURS100). Direct compression technique was used to prepare coated tablets while matrix tablets were prepared by wet granulation and direct compression methods. The prepared formulations were evaluated in terms of their precompression parameters, physical characteristics, dissolution test and in vitro drug release kinetic studies. The results showed that matrix tablets containing 7.5or10% of EuRS100 and EuRL100 respectively and that coated tablets prepared by using coating solution (15%) which was applied about 120(in case of EuRS100) or 280 (in case of EuRL100) times were the best. These tablets released about 90-95% of verapamil within 24h
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