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تسجيل مستخدم جديدHot isostatic pressing of powder in tube MgB2 wires
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The critical current density (Jc) of hot isostatic pressed (HIPed) MgB2 wires, measured by d.c. transport and magnetization, is compared with that of similar wires annealed at ambient pressure. The HIPed wires have a higher Jc than the annealed wires, especially at high temperatures and magnetic fields, and higher irreversibility field (Hirr). The HIPed wires are promising for applications, with Jc>106 A/cm2 at 5 K and zero field and >104 A/cm2 at 1.5 T and 26.5 K, and Hirr ~ 17 T at 4 K. The improvement is attributed to a high density of structural defects, which are the likely source of vortex pinning. These defects, observed by transmission electron microscopy, include small angle twisting, tilting, and bending boundaries, resulting in the formation of sub-grains within MgB2 crystallites.
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The microstructures of MgB2 wires prepared by the powder-in-tube technique and subsequent hot isostatic pressing were investigated using transmission electron microscopy. Large amount of crystalline defects including small angle twisting, tilting, an
d bending boundaries, in which high densities of dislocations reside, were found forming sub-grains within MgB2 grains. It is believed that these defects resulted from particle deformation during the hot isostatic pressing process and are effective flux pinning centers that contribute to the high critical current densities of the wires at high temperatures and at high fields.
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