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Register a new userInsight into bulk niobium superconducting RF cavities performances by tunneling spectroscopy
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Point contact tunneling (PCT) spectroscopy measurements are reported over wide areas of cm-sized cut outs from niobium superconducting RF cavities. A comparison is made between a high-quality, conventionally processed (CP) cavity with a high field Q drop for acceleration field E $>$ 20 MV/m and a nitrogen doped (N-doped) cavity that exhibits an increasing Q up to fields approaching 15 MV/m. The CP cavity displays hot spot regions at high RF fields where Q-drop occurs as well as unaffected regions (cold spots). PCT data on cold spots reveals a near ideal BCS density of states (DOS) with gap parameters, $Delta$ as high as 1.62 meV, that are among the highest values ever reported for Nb. Hot spot regions exhibit a wide distribution of gap values down to $Delta sim$ 1.0 meV and DOS broadening characterized by a relatively large value of pair-breaking rate, $Gamma$, indicating surface regions of significantly reduced superconductivity. In addition, hot spots commonly exhibit Kondo tunneling peaks indicative of surface magnetic moments attributed to a defective oxide. N-doped cavities reveal a more homoegeneous gap distribution centered at $Delta sim$ 1.5 meV and relatively small values of $Gamma/Delta$. The absence of regions of significantly reduced superconductivity indicates that the N interstitials are playing an important role in preventing the formation of hydride phases and other macroscopic defects which might otherwise severely affect the local, surface superconductivity that lead to hot spot formation. The N-doped cavities also display a significantly improved surface oxide, i.e., increased thickness and tunnel barrier height, compared to CP cavities. These results help explain the improved performance of N-doped cavities and give insights into the origin of the initial increasing Q with RF amplitude.
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A systematic study is presented on the superconductivity (sc) parameters of the ultrapure niobium used for the fabrication of the nine-cell 1.3 GHz cavities for the linear collider project TESLA. Cylindrical Nb samples have been subjected to the same surface treatments that are applied to the TESLA cavities: buffered chemical polishing (BCP), electrolytic polishing (EP), low-temperature bakeout (LTB). The magnetization curves and the complex magnetic susceptibility have been measured over a wide range of temperatures and dc magnetic fields, and also for di erent frequencies of the applied ac magnetic field. The bulk superconductivity parameters such as the critical temperature Tc = 9.26 K and the upper critical field Bc2(0) = 410 mT are found to be in good agreement with previous data. Evidence for surface superconductivity at fields above Bc2 is found in all samples. The critical surface field exceeds the Ginzburg-Landau field Bc3 = 1.695Bc2 by about 10% in BCP-treated samples and increases even further if EP or LTB are applied. From the field dependence of the susceptibility and a power-law analysis of the complex ac conductivity and resistivity the existence of two different phases of surface superconductivity can be established which resemble the Meissner and Abrikosov phases in the bulk: (1) coherent surface superconductivity, allowing sc shielding currents flowing around the entire cylindrical sample, for external fields B in the range between Bc2 and Bcohc3, and (2) incoherent surface superconductivity with disconnected sc domains between Bcohc3 and Bc3. The coherent critical surface field separating the two phases is found to be Bcoh c3 = 0.81Bc3 for all samples. The exponents in the power law analysis are different for BCP and EP samples, pointing to different surface topologies.
We study mechanisms of vortex nucleation in Nb$_3$Sn Superconducting RF (SRF) cavities using a combination of experimental, theoretical, and computational methods. Scanning transmission electron microscopy (STEM) image and energy dispersive spectroscopy (EDS) of some Nb$_3$Sn cavities show Sn segregation at grain boundaries in Nb$_3$Sn with Sn concentration as high as $sim$35 at.% and widths $sim$3 nm in chemical composition. Using ab initio calculations, we estimate the effect excess tin has on the local superconducting properties of the material. We model Sn segregation as a lowering of the local critical temperature. We then use time-dependent Ginzburg-Landau theory to understand the role of segregation on magnetic vortex nucleation. Our simulations indicate that the grain boundaries act as both nucleation sites for vortex penetration and pinning sites for vortices after nucleation. Depending on the magnitude of the applied field, vortices may remain pinned in the grain boundary or penetrate the grain itself. We estimate the superconducting losses due to vortices filling grain boundaries and compare with observed performance degradation with higher magnetic fields. We estimate that the quality factor may decrease by an order of magnitude ($10^{10}$ to $10^9$) at typical operating fields if 0.03% of the grain boundaries actively nucleate vortices. We additionally estimate the volume that would need to be filled with vortices to match experimental observations of cavity heating.
In this work we investigate superconducting properties of niobium samples via application of the muon spin rotation/relaxation (muSR) technique. We employ for the first time the muSR technique to study samples that are cutout from large and small grain 1.5 GHz radio frequency (RF) single cell niobium cavities. The RF test of these cavities was accompanied by full temperature mapping to characterize the RF losses in each of the samples. Results of the muSR measurements show that standard cavity surface treatments like mild baking and buffered chemical polishing (BCP) performed on the studied samples affect their surface pinning strength. We find an interesting correlation between high field RF losses and field dependence of the sample magnetic volume fraction measured via muSR. The muSR line width observed in ZF-muSR measurements matches the behavior of Nb samples doped with minute amounts of Ta or N impurities. An upper bound for the upper critical field Hc2 of these cutouts is found.
Point contact tunneling (PCT) and low energy muon spin rotation (LE-muSR) are used to probe, on the same samples, the surface superconducting properties of micrometer thick niobium films deposited onto copper substrates using different sputtereing techniques: diode, dc magnetron (dcMS) and HIPIMS. The combined results are compared to radio-frequency tests performances of RF cavities made with the same processes. Degraded surface superconducting properties are found to yield lower quality factors and stronger Q slope. In addition, both techniques find evidence for surface paramagnetism on all samples and particularly on Nb films prepared by HIPIMS.
It is shown that in a structure consisting of a superconducting ring-shaped electrode overlapped by a normal metal contact through a thin oxide barrier, measurements of the tunnel current in magnetic field can probe persistent currents in the ring. The effect manifests itself as periodic oscillations of the tunnel current through the junction at a fixed bias voltage as function of perpendicular magnetic field. The magnitude of oscillations depends on bias point. It reaches maximum at energy eV which is close to the superconducting gap and decreases with increase of temperature. The period of oscillations dF in units of magnetic flux is equal neither to h/e nor to h/2e, but significantly exceeds these values for larger loop circumferences. The phenomenon is explained by formation of metastable states with large vorticity. The pairing potential and the superconducting density of states are periodically modulated by the persistent currents at sub-critical values resulting in corresponding variations of the measured tunnel current.
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