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Register a new userA low energy muon spin rotation and point contact tunneling study of niobium films prepared for superconducting cavities
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T. Junginger
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Point contact tunneling (PCT) and low energy muon spin rotation (LE-muSR) are used to probe, on the same samples, the surface superconducting properties of micrometer thick niobium films deposited onto copper substrates using different sputtereing techniques: diode, dc magnetron (dcMS) and HIPIMS. The combined results are compared to radio-frequency tests performances of RF cavities made with the same processes. Degraded surface superconducting properties are found to yield lower quality factors and stronger Q slope. In addition, both techniques find evidence for surface paramagnetism on all samples and particularly on Nb films prepared by HIPIMS.
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In this work we investigate superconducting properties of niobium samples via application of the muon spin rotation/relaxation (muSR) technique. We employ for the first time the muSR technique to study samples that are cutout from large and small grain 1.5 GHz radio frequency (RF) single cell niobium cavities. The RF test of these cavities was accompanied by full temperature mapping to characterize the RF losses in each of the samples. Results of the muSR measurements show that standard cavity surface treatments like mild baking and buffered chemical polishing (BCP) performed on the studied samples affect their surface pinning strength. We find an interesting correlation between high field RF losses and field dependence of the sample magnetic volume fraction measured via muSR. The muSR line width observed in ZF-muSR measurements matches the behavior of Nb samples doped with minute amounts of Ta or N impurities. An upper bound for the upper critical field Hc2 of these cutouts is found.
Point contact tunneling (PCT) spectroscopy measurements are reported over wide areas of cm-sized cut outs from niobium superconducting RF cavities. A comparison is made between a high-quality, conventionally processed (CP) cavity with a high field Q drop for acceleration field E $>$ 20 MV/m and a nitrogen doped (N-doped) cavity that exhibits an increasing Q up to fields approaching 15 MV/m. The CP cavity displays hot spot regions at high RF fields where Q-drop occurs as well as unaffected regions (cold spots). PCT data on cold spots reveals a near ideal BCS density of states (DOS) with gap parameters, $Delta$ as high as 1.62 meV, that are among the highest values ever reported for Nb. Hot spot regions exhibit a wide distribution of gap values down to $Delta sim$ 1.0 meV and DOS broadening characterized by a relatively large value of pair-breaking rate, $Gamma$, indicating surface regions of significantly reduced superconductivity. In addition, hot spots commonly exhibit Kondo tunneling peaks indicative of surface magnetic moments attributed to a defective oxide. N-doped cavities reveal a more homoegeneous gap distribution centered at $Delta sim$ 1.5 meV and relatively small values of $Gamma/Delta$. The absence of regions of significantly reduced superconductivity indicates that the N interstitials are playing an important role in preventing the formation of hydride phases and other macroscopic defects which might otherwise severely affect the local, surface superconductivity that lead to hot spot formation. The N-doped cavities also display a significantly improved surface oxide, i.e., increased thickness and tunnel barrier height, compared to CP cavities. These results help explain the improved performance of N-doped cavities and give insights into the origin of the initial increasing Q with RF amplitude.
We have performed depth dependent muon spin rotation/relaxation studies of the dynamics of single layer films of {it Au}Fe and {it Cu}Mn spin glasses as a function of thickness and of its behavior as a function of distance from the vacuum interface (5-70 nm). A significant reduction in the muon spin relaxation rate as a function of temperature with respect to the bulk material is observed when the muons are stopped near (5-10 nm) the surface of the sample. A similar reduction is observed for the whole sample if the thickness is reduced to e.g. 20 nm and less. This reflects an increased impurity spin dynamics (incomplete freezing) close to the surface although the freezing temperature is only modestly affected by the dimensional reduction.
Point-contact (PC) Andreev-reflection (AR) measurements of the superconducting gap in iron-oxipnictide ReFeAsO_{1-x}F_x (Re=La, Sm) films have been carried out. The value of the gap is distributed in the range 2Delta simeq 5-10 meV (for Re=Sm) with a maximum in the distribution around 6 meV. Temperature dependence of the gap Delta(T) can be fitted well by BCS curve giving reduced gap ratio 2Delta /kT_c^*simeq 3.5 (here T_c^* is the critical temperature from the BCS fit). At the same time, an expected second larger gap feature was difficult to resolve distinctly on the AR spectra making determination reliability of the second gap detection questionable. Possible reasons for this and the origin of other features like clear-cut asymmetry in the AR spectra and current regime in PCs are discussed.
Muon spin rotation (muSR) experiments were performed on the intercalated graphite CaC6 in the normal and superconducting state down to 20 mK. In addition, AC magnetization measurements were carried out resulting in an anisotropic upper critical field Hc2, from which the coherence lengths xi_ab(0)=36.3(1.5) nm and xi_c(0)=4.3(7) nm were estimated. The anisotropy parameter gamma_H= H_c2_ab/H_c2_c increases monotonically with decreasing temperature. A single isotropic s-wave description of superconductivity cannot account for this behaviour. From magnetic field dependent muSR experiments the absolute value of the in-plane magnetic penetretion depth lambda_ab=78(3) nm was determined. The temperature dependence of the superfluid density rho_s(T) is slightly better described by a two-gap than a single-gap model.
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