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Register a new userMuon spin rotation studies of niobium for superconducting RF applications
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In this work we investigate superconducting properties of niobium samples via application of the muon spin rotation/relaxation (muSR) technique. We employ for the first time the muSR technique to study samples that are cutout from large and small grain 1.5 GHz radio frequency (RF) single cell niobium cavities. The RF test of these cavities was accompanied by full temperature mapping to characterize the RF losses in each of the samples. Results of the muSR measurements show that standard cavity surface treatments like mild baking and buffered chemical polishing (BCP) performed on the studied samples affect their surface pinning strength. We find an interesting correlation between high field RF losses and field dependence of the sample magnetic volume fraction measured via muSR. The muSR line width observed in ZF-muSR measurements matches the behavior of Nb samples doped with minute amounts of Ta or N impurities. An upper bound for the upper critical field Hc2 of these cutouts is found.
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Point contact tunneling (PCT) and low energy muon spin rotation (LE-muSR) are used to probe, on the same samples, the surface superconducting properties of micrometer thick niobium films deposited onto copper substrates using different sputtereing techniques: diode, dc magnetron (dcMS) and HIPIMS. The combined results are compared to radio-frequency tests performances of RF cavities made with the same processes. Degraded surface superconducting properties are found to yield lower quality factors and stronger Q slope. In addition, both techniques find evidence for surface paramagnetism on all samples and particularly on Nb films prepared by HIPIMS.
Measurements of the in-plane magnetic field penetration depth lambda_{ab} in Fe-based superconductors with the nominal composition SmFeAsO_0.85 (T_csimeq52K) and NdFeAsO_0.85 (T_csimeq51K) were carried out by means of muon-spin-rotation. The absolute values of lambda_{ab} at T=0 were found to be 189(5)nm and 195(5)nm for Sm and Nd substituted samples, respectively. The analysis of the magnetic penetration depth data within the Uemura classification scheme, which considers the correlation between the superconducting transition temperature T_c and the effective Fermi temperature T_F, reveal that both families of Fe-based superconductors (with and without fluorine) falls to the same class of unconventional superconductors.
In a recent article Tran et al. [Phys. Rev.B 78, 172505 (2008)] report on the result of the muon-spin rotation (muSR) measurements of Mo_3Sb_7 superconductor. Based on the analysis of the temperature and the magnetic field dependence of the Gaussian relaxation rate sigma_{sc} they suggest that Mo_3Sb_7 is the superconductor with two isotropic s-wave like gaps. An additional confirmation was obtained from the specific heat data published earlier by partly the same group of authors in [Acta Mater. 56, 5694 (2008)]. The purpose of this Comment is to point out that from the analysis made by Tran et al. the presence of two superconducting energy gaps in Mo_3Sb_7 can not be justified. The analysis of muSR data does not account for the reduction of sigma_{sc} with increasing temperature, and, hence, yields inaccurate information on the magnetic penetration depth. The specific heat data can be satisfactory described within the framework of the one-gap model with the small residual specific heat component. The experimental data of Tran et al., as well as our earlier published muSR data [Phys. Rev. B 78, 014502 (2008)] all seem to be consistent with is the presence of single isotropic superconducting energy gap in Mo_3Sb_7.
Point contact tunneling (PCT) spectroscopy measurements are reported over wide areas of cm-sized cut outs from niobium superconducting RF cavities. A comparison is made between a high-quality, conventionally processed (CP) cavity with a high field Q drop for acceleration field E $>$ 20 MV/m and a nitrogen doped (N-doped) cavity that exhibits an increasing Q up to fields approaching 15 MV/m. The CP cavity displays hot spot regions at high RF fields where Q-drop occurs as well as unaffected regions (cold spots). PCT data on cold spots reveals a near ideal BCS density of states (DOS) with gap parameters, $Delta$ as high as 1.62 meV, that are among the highest values ever reported for Nb. Hot spot regions exhibit a wide distribution of gap values down to $Delta sim$ 1.0 meV and DOS broadening characterized by a relatively large value of pair-breaking rate, $Gamma$, indicating surface regions of significantly reduced superconductivity. In addition, hot spots commonly exhibit Kondo tunneling peaks indicative of surface magnetic moments attributed to a defective oxide. N-doped cavities reveal a more homoegeneous gap distribution centered at $Delta sim$ 1.5 meV and relatively small values of $Gamma/Delta$. The absence of regions of significantly reduced superconductivity indicates that the N interstitials are playing an important role in preventing the formation of hydride phases and other macroscopic defects which might otherwise severely affect the local, surface superconductivity that lead to hot spot formation. The N-doped cavities also display a significantly improved surface oxide, i.e., increased thickness and tunnel barrier height, compared to CP cavities. These results help explain the improved performance of N-doped cavities and give insights into the origin of the initial increasing Q with RF amplitude.
We present an analysis of the Nb3Sn surface layers grown on a bulk niobium (Nb) coupon prepared at the same time and by the same vapor diffusion process used to make Nb3Sn coatings on 1.3 GHz cavities. Tunneling spectroscopy reveals a well-developed, homogeneous superconducting density of states at the surface with a gap value distribution centered around 2.7 meV and superconducting critical temperature (Tc) up to 16.3 K. Scanning Electron microscopy (STEM) performed on cross section of the samples surface region shows a 2 microns thick Nb3Sn surface layer. The elemental composition map exhibits a Nb over Sn ratio of 3 and reveals the presence of buried sub-stoichiometric regions that have a ratio f 5. Synchrotron x-ray diffraction experiments indicate a polycrystalline Nb3Sn film and confirm the presence of Nb rich regions that occupy about a third of the coating volume. These low Tc regions could play an important role in the dissipation mechanism occurring during RF tests of Nb3Sn-coated cavities and open the way for further improving a very promising alternative to pure Nb cavities for particle accelerators.
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