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In this study, we use our recently prepared graphene oxide (GO) with an almost intact {sigma}-framework of C-atoms (ai-GO) to probe the thermal stability of the carbon framework for the first time. Ai-GO exhibits few defects only by preventing CO2 formation during synthesis. Ai-GO was thermally treated before chemical reduction and subsequently the resulting defect density in graphene was determined by statistical Raman microscopy. Surprisingly, the carbon framework of ai-GO is stable in thin films up to 100 {deg}C. Furthermore, we find evidence for an increasing quality of ai-GO upon annealing at 50 {deg}C before reduction. The carbon framework of GO prepared according to the popular Hummers method (GO-c)appears to be less stable and decomposition starts at 50 {deg}C what is qualitatively indicated by CO2-trapping experiments in {mu}m-thin films. Information about the stability of GO is important for storing, processing and applying GO in applications.
The solid electrolyte interphase (SEI) is detrimental for rechargeable batteries performance and lifetime. Understanding its formation requires analytical techniques that provide molecular level insight. Here dynamic nuclear polarization (DNP) is uti
The sorption of radionuclides by graphene oxides synthesized by different methods was studied through a combination of batch experiments with characterization by microscopic and spectroscopic techniques such as X-ray photoelectron spectroscopy (XPS),
Chlorinated hydrocarbon compounds are of environmental concerns, since they are toxic to humans and other mammals, are widespread, and exposure is hard to avoid. Understanding and improving methods to reduce the amount of the substances is important.
We present the results of an experiment on measuring the gradient of the Casimir force between an Au-coated hollow glass microsphere and graphene-coated fused silica plate by means of a modified atomic force microscope cantilever based technique oper
We present the results of the characterization of Mg/Co periodic multilayers and their thermal stability for the EUV range. The annealing study is performed up to a temperature of 400degree C. Images obtained by scanning transmission electron microsc