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Register a new userA Series of Plasma Innovation Technologies by Double Glow Discharge Phenomenon
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In order to break the limitation of plasma nitriding technology,which can be applied to a few nonmetallic gaseous elements, the Double Glow Discharge Phenomenon was found and then invented the Double Glow Plasma Surface Metallurgy Technology. This double glow plasma surface metallurgy technology can use any element in the periodic table of chemical elements for surface alloying of metal materials. Countless surface alloys with special physical and chemical properties have been produced on the surfaces of conductive materials.By using double glow discharge phenomenon,a series of new plasma technologies,such as the double glow plasma graphene technology, double glow plasma brazing technology,double glow plasma sintering technology, double glow plasma nanotechnology,double glow plasma cleaning technology, double glow plasma carburizing without hydrogen and so on, have been invented.A very simple phenomenon of double glow discharge can generate about 10 plasma innovation technologies, which fully shows that there is still a lot of innovation space on the basis of classical physics.This paper briefly introduces the basic principles,functions and characteristics of each technology. The application prospects and development directions of plasma in metal materials and machinery manufacturing industry will also be discussed.
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Plasma Surface Metallurgy/Alloying is a kind of surface metallurgy/alloying to employ low temperature plasma produced by glow discharge to diffuse alloying elements into the surface of substrate material to form an alloy layer. The first plasma surface metallurgy technology is plasma nitriding invented by German scientist Dr. Bernard Berghuas in 1930. He was the first person to apply glow discharge to realize the surface alloying. In order to break the limitation of plasma nitriding technology, which can only be applied to a few non-metallic gaseous elements such as nitrogen, carbon, sulfur, the Double Glow Discharge Phenomenonwas found in 1978. Based on this phenomenon the Double Glow Plasma Surface Metallurgy Technology, also known as the Xu-Tec Process was invented in 1980. It can utilize any chemical elements in the periodic table including solid metallic, gas non-metallic elements and their combination to realize plasma surface alloying, hence greatly expanded the field of surface alloying. Countless surface alloys with high hardness, wear resistance and corrosion resistance, such as high speed steels, nickel base alloys and burn resistant alloys have been produced on the surfaces of a variety of materials. This technology may greatly improve the surface properties of metal materials, comprehensively improve the quality of mechanical products, save a lot of precious alloy elements for human beings. Based on the plasma nitriding technology, the Xu-Tec Process has opened up a new material engineering field of Plasma Surface Metallurgy. This Review Article briefly presents the history of glow discharge and surface alloying, double glow discharge phenomenon, basic principle and current status of Double Glow Plasma Surface Metallurgy/Alloying. Industrial applications, advantages and future potential of the Xu-Tec process are also presented.
Highly Oriented Pyrolytic Graphite was exfoliated via pulsed discharge plasma in liquid nitrogen. The potential mechanisms involved were investigated by observing the treated surface of the graphitic material and the obtained particles. Non-exfoliating defects from the plasma treatment were observed and experimental parameter were modified to counteract those. One experiment was performed without exposing the HOPG directly to the discharges so as to better understand the plasma role. The exfoliated particles were observed via TEM and SEM to evaluate the defects, the size, the purity and the crystallinity but no quantitative characterization of their thickness was possible so the actual number of layer of each particle is unknown. Nonetheless, few layers graphene (FLG) was successfully exfoliated through this process. The proposed mechanisms were extrapolated from the observation of the damaged HOPG surface and the obtained particles but the correlation found does not prove causation.
In this paper non-linear dynamics of a periodically forced excitable glow discharge plasma has been studied. The experiments were performed in glow discharge plasma where excitability was achieved for suitable discharge voltage and gas pressure. The plasma was first perturbed by a sub-threshold sawtooth periodic signal, and we obtained small sub-threshold oscillations. These oscillations showed resonance when the frequency of the perturbation was around the characteristic frequency the plasma, and hence may be useful to estimate characteristic of an excitable system. On the other hand, when the perturbation was supra-threshold, system showed frequency entrainments. We obtained harmonic frequency entrainments for perturbation frequency greater than the characteristic frequency of the system and for lesser than the characteristic frequency, system showed only excitable behaviour.
Plasmas at atmospheric pressure are presented as a simple, fast, and versatile tool for the synthesis or/and the grafting of noble metallic NPs (Au, Pt) on substrates. In this study, noble metal NPs are generated either by the reduction of a gold salt in an aqueous medium by microplasma or either by the decomposition of a platinum or gold organometallic in the post-discharge of an atmospheric plasma torch. The latter can also be used for the grafting of NPs from a commercial colloidal solution
The electron sheath formation in a DC magnetised plasma of modified hollow cathode source is studied. The discharge consists of two plane parallel cathodes and a small cubical anode placed off axis at the center. The argon plasma is produced and the properties of the plasma in response to the sheath formation near the anode are studied using electrical and optical diagnostics. In particular, the effect of pressure, magnetic field on discharge parameters such as discharge current, plasma potential, plasma density and electron temperature is studied. The discharge showed an onset of anode glow at a critical applied magnetic field indicating the formation of electron sheath and a double layer. The discharge current initially decreases; however it starts to rise again as the anode spot appears on the anode. The critical magnetic field at which anode glow formation takes place is dependent upon operating pressure and discharge voltage. The transition from ion sheath to electron sheath is investigated in detail by Langmuir probe and spectroscopy diagnostics. The plasma potential near the anode decreases during the transition from ion sheath to electron sheath. The plasma potential locks to the ionization potential of argon gas when anode spot is completely formed. A systematic study showed that during the transition, the electron temperature increases and plasma density decreases in the bulk plasma. The spectroscopy of the discharge showed presence of strong atomic and ionic lines of argon. The intensity of these spectral lines showed a dip during the transition between two sheaths. After the formation of the anode spot, oscillations of the order of 5-20 kHz are observed in the discharge current and floating potential due to the enhanced ionisation and excitation processes in the electron sheath.
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