In This Research Studied The solubility of Succinic acid in water +
THF mixtures by astatic analytical technique using the acid–base
titration method at temperatures ranging from 298.15 to 333.15 K
and atmospheric pressure.
Tow compounds have been synthesised: tetra butyl ammonium
alginate and dodecanoate sodium alginate ester.
The synthesis of compound (1) by transferring
sodium alginate to Alginic acid and then adjusted by tetra-butyl
ammonium hydroxide. The comp
ound (2) was synthesised from
tetra-butyl ammonium alginate according to Fisherest erification,
between tetra-butylammonium alginate and dodecanoic acid and
using (Amberlyst-15) as a hetrogeneous acid catalyst, and then the
product react with sodium carbonate.
The aim of this research is to study the most important physical, chemical and
microbial changes in several kinds of infant milk available in local markets. The milk
samples were studied in conditions similar to those used by mothers when they prep
are
infant milk bottles at their houses. The results showed that moisture content increased in all
samples from approximately 1% to 3.2-4.4% after storage for 9 days. Acidity increased
considerably from 0.14% to 0.2%.
The results showed that peroxide value passed the allowable limits (0.25) and
reached about (0.47) in samples stored for 9 days at room temperature. However, the value
for samples stored in the refrigerator ranged between (0.25-0.29). The free acidity number
of fat for all samples specially the refrigerated ones was within the natural limits (<0.5).
Chromatographic analyses showed apparent differences in fatty acid percentages between
the kinds of milk. The rate of lenoleic acid (C 18-2 ) decreased during storage in all samples
and in all conditions.
Soluble nitrogen increased in all samples at the end of storage and the highest value
was 0.49% in Nido milk samples. The solubility of milk samples was checked during
storage and was found to decrease very little ( 1%).
The total count of aerobic bacteria showed that all samples conform to the Syrian
standards (No. 197, 1996) during the first six days of storage, but they passed the upper
limits at the end of storage. However, all samples were free of pathogenic microbes .
A pot experiment was conducted to evaluate the relative agronomic
effectiveness (RAE%) of a Syrian phosphate rock when it is added alone and as
mixture with elemental sulfur with three different ratios (PR:S) (2:1) (5:1) (8:1)
and compared with tr
iple superphosphate. The main results of this study
showed that Ain Layloun phosphate rock was not effective for direct use by
Rye grass when used alone, but it became effective when mixed with elemental
sulfur. The relative agronomic effectiveness was varied following mixing ratios,
it was 50%, 76% and 87% in (8:1), (5:1) and (2:1) (PR:S) mixing ratios
respectively. This is due to the increase of available soil phosphorus content
which is related to the increase of phosphate rock solubility due to decrease of
pH derived from oxidation of sulfur by Thiobacillus spp.