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High-quality superconducting KxFeySe2 single crystals were synthesized using an easy one-step method. Detailed annealing studies were performed to make clear the phase formation process in KxFeySe2. Compatible observations were found in temperature-dependent X-ray diffraction patterns, back-scattered electron images and corresponding electromagnetic properties, which proved that good superconductivity performance was close related to the microstructure of superconducting component. Analysis based on the scaling behavior of flux pinning force indicated that the dominant pinning mechanism was delta(Tc) pinning and independent of connectivity. The annealing dynamics studies were also performed, which manifested that the humps in temperature-dependent resistance (RT) curves were induced by competition between the metallic/superconducting and the semiconducting/insulating phases.
Here, we report the synthesis and characterization of sulphur-substituted iron telluride i.e. FeTe1-xSx; (x = 0-30 %) system and study the impact of low temperature oxygen (O2) annealing as well. Rietveld analysis of room temperature x-ray diffractio
We discovered a novel annealing method for Fe-chalcogenide superconductors. It was found that sulfur annealing deintercalated excess Fe via formation of FeS2. Due to its specifics, sulfur annealing is applicable when preparing Fe-chalcogenide-based wires or cables.
The effect of damage induced by 2-MeV alpha particles, followed by annealing, on the critical temperature (Tc), resistivity, and upper critical field (Hc2), of three MgB2 films made by different deposition processes has been studied. Damage creates a
We report an easy single step synthesis route of title compound NdFeAsO0.80F0.20 superconductor having bulk superconductivity below 50 K. The title compound is synthesized via solid-state reaction route by encapsulation in an evacuated (10-3 Torr) qu
We report successful growth of flux free large single crystals of superconducting FeSe1/2Te1/2 with typical dimensions of up to few cm. The AC and DC magnetic measurements revealed the superconducting transition temperature (Tc) value of around 11.5K