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Electron irradiation is investigated as a way to dope the topological insulator Bi2Te3. For this, p-type Bi2Te3 single crystals have been irradiated with 2.5 MeV electrons at room temperature and electrical measurements have been performed in-situ as well as ex-situ in magnetic fields up to 14 T. The defects created by irradiation act as electron donors allowing the compensation of the initial hole-type conductivity of the material as well as the conversion of the conductivity from p- to n-type. The changes in carrier concentration are investigated using Hall effect and Shubnikov-de Haas (SdH) oscillations, clearly observable in the p-type samples before irradiation, but also after the irradiation-induced conversion of the conductivity to n-type. The SdH patterns observed for the magnetic field along the trigonal axis can be entirely explained assuming the contribution of only one valence and conduction band, respectively, and Zeeman-splitting of the orbital levels.
154 - B. Leridon , P. Monod , D. Colson 2009
We present here high precision magnetisation measurements in polycrystalline $YBa_2Cu_3O_{x}$ samples, with oxygen content ranging from $x=6.19$ to $x=7.00$. By analysing the temperature derivative of the susceptibility, we found in the underdoped su perconducting samples a singular point at a temperature corresponding to $T_{mag}$, the temperature below which polarised neutrons experiments have evidenced a symmetry breaking. We believe that this is a thermodynamic indication for the existence of a phase transition in the pseudogap state of underdoped $YBa_2Cu_3O_{x}$.
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