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Critical-angle x-ray transmission grating spectrometer with extended bandpass and resolving power > 10,000

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 Added by Ralf Heilmann
 Publication date 2016
  fields Physics
and research's language is English




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Several high priority subjects in astrophysics can be addressed by a state-of-the-art soft x-ray grating spectrometer (XGS). An Explorer-scale, large-area (> 1,000 cm2), high resolving power (R > 3,000) XGS is highly feasible based on Critical-Angle Transmission (CAT) gratings, even for telescopes with angular resolution of 5-10 arcsec. Significantly higher performance can be provided by a CAT XGS on an X-ray-Surveyor-type mission. CAT gratings combine the advantages of blazed reflection gratings (high efficiency, use of higher diffraction orders) with those of transmission gratings (low mass, relaxed alignment and temperature requirements, transparent at high energies) with minimal mission resource demands. They are high-efficiency blazed transmission gratings that consist of freestanding, ultra-high aspect-ratio grating bars made from SOI wafers using anisotropic dry and wet etch techniques. Blazing is achieved through reflection off grating bar sidewalls. Silicon is well matched to the soft x-ray band, and existing silicon CAT gratings exceed 30% absolute diffraction efficiency, with clear paths for improvement. CAT gratings coated with heavier elements allow extension of the CAT grating principle to higher energies and larger angles, enabling higher resolving power at shorter wavelengths. We show x-ray data from CAT gratings coated with platinum using atomic layer deposition, and demonstrate blazing to higher energies and much larger blaze angles than possible with silicon. We measure resolving power of a CAT XGS consisting of a Wolter-I focusing mirror pair from GSFC and CAT gratings, performed at the MSFC SLF. Measurement of the Al Ka doublet in 18th order shows resolving power > 10,000, based on preliminary analysis. This demonstrates that currently fabricated CAT gratings are compatible with the most advanced XGS designs for future soft x-ray spectroscopy missions.



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We present measurements of the resolving power of a soft x-ray spectrometer consisting of 200 nm-period lightweight, alignment-insensitive critical-angle transmission (CAT) gratings and a lightweight slumped-glass Wolter-I focusing mirror pair. We measure and model contributions from source, mirrors, detector pixel size, and grating period variation to the natural line width spectrum of the Al and Mg K$_{alpha_1 alpha_2}$ doublets. Measuring up to 18$^{rm th}$ diffraction order at characteristic Al-K wavelengths we consistently obtain small broadening due to gratings corresponding to a minimum effective grating resolving power $R_g > 10,000$ with 90% confidence. Upper limits are often compatible with $R_g = infty$. Independent fitting of different diffraction orders, as well as ensemble fitting of multiple orders at multiple wavelengths, gives compatible results. Our data leads to uncertainties for the Al-K$_{alpha}$ doublet line width and line separation parameters 2-3 times smaller than values found in the literature. Data from three different gratings are mutually compatible. This demonstrates that CAT gratings perform in excess of the requirements for the Arcus Explorer mission and are suitable for next-generation space-based x-ray spectrometer designs with resolving power 5-10 times higher than the transmission grating spectrometer on the Chandra X-ray Observatory.
High-resolution ($R = lambda /Delta lambda > 2000$) x-ray absorption and emission line spectroscopy in the soft x-ray band is a crucial diagnostic for the exploration of the properties of ubiquitous warm and hot plasmas and their dynamics in the cosmic web, galaxy clusters, galaxy halos, intragalactic space, and star atmospheres. Soft x-ray grating spectroscopy with $R > 10{,}000$ has been demonstrated with critical-angle transmission (CAT) gratings. CAT gratings combine the relaxed alignment and temperature tolerances and low mass of transmission gratings with high diffraction efficiency blazed in high orders. They are an enabling technology for the proposed Arcus grating explorer and were selected for the Lynx design reference mission grating spectrometer instrument. Both Arcus and Lynx require the manufacture of hundreds to perhaps $approx 2000$ large-area CAT gratings. We are developing new patterning and fabrication process sequences that are conducive to large-format volume processing on state-of-the-art 200 mm wafer tools. Recent x-ray tests on 200 nm-period gratings patterned using e-beam-written masks and 4x projection lithography in conjunction with silicon pore focusing optics demonstrated $R approx 10^4$ at 1.49 keV. Extending the grating depth from 4 $mu$m to 6 $mu$m is predicted to lead to significant improvements in diffraction efficiency and is part of our current efforts using a combination of deep reactive-ion etching and wet etching in KOH solution. We describe our recent progress in grating fabrication and report our latest diffraction efficiency and modeling results.
The Mid-Infrared Instrument (MIRI) on-board JWST will provide imaging, coronagraphy, low-resolution spectroscopy and medium-resolution spectroscopy at unprecedented sensitivity levels in the mid-infrared wavelength range. The Medium-Resolution Spectrometer (MRS) of MIRI is an integral field spectrograph that provides diffraction-limited spectroscopy between 4.9 and 28.3 um, within a FOV varying from 13 to 56 square. From ground testing, we calculate the physical parameters essential to general observers and calibrating the wavelength solution and resolving power of the MRS is critical for maximising the scientific performance of the instrument. We have used ground-based observations of discrete spectral features in combination with Fabry-Perot etalon spectra to characterize the wavelength solution and spectral resolving power of the MRS. We present the methodology used to derive the MRS spectral characterisation, which includes the precise wavelength coverage of each MRS sub-band, computation of the resolving power as a function of wavelength, and measuring slice-dependent spectral distortions. The resolving power varies from R3500 in channel 1 to R1500 in channel 4. Based on the ground test data, the wavelength calibration accuracy is estimated to be below one tenth of a pixel, with small systematic shifts due to the target position within a slice for unresolved sources, that have a maximum amplitude of about 0.25 spectral resolution elements. Based on ground test data, the MRS complies with the spectral requirements for both the R and wavelength accuracy for which it was designed. We also present the commissioning strategies and targets that will be followed to update the spectral characterisation of the MRS.
A new type of hemispherical electron energy analyzer that permits angle and spin resolved photoelectron spectroscopy has been developed. The analyzer permits standard angle resolved spectra to be recorded with a two-dimensional detector in parallel with spin detection using a mini-Mott polarimeter. General design considerations as well as technical solutions are discussed and test results from the Au(111) surface state are presented.
We present the first X-ray spectrum obtained by the Low Energy Transmission Grating Spectrometer (LETGS) aboard the Chandra X-ray Observatory. The spectrum is of Capella and covers a wavelength range of 5-175 A (2.5-0.07 keV). The measured wavelength resolution, which is in good agreement with ground calibration, is $Delta lambda simeq$ 0.06 A (FWHM). Although in-flight calibration of the LETGS is in progress, the high spectral resolution and unique wavelength coverage of the LETGS are well demonstrated by the results from Capella, a coronal source rich in spectral emission lines. While the primary purpose of this letter is to demonstrate the spectroscopic potential of the LETGS, we also briefly present some preliminary astrophysical results. We discuss plasma parameters derived from line ratios in narrow spectral bands, such as the electron density diagnostics of the He-like triplets of carbon, nitrogen, and oxygen, as well as resonance scattering of the strong Fe XVII line at 15.014 A.
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