The recently confirmed neutron-shell closure at N = 32 has been investigated for the first time below the magic proton number Z = 20 with mass measurements of the exotic isotopes 52,53K, the latter being the shortest-lived nuclide investigated at the
online mass spectrometer ISOLTRAP. The resulting two-neutron separation energies reveal a 3 MeV shell gap at N = 32, slightly lower than for 52Ca, highlighting the doubly-magic nature of this nuclide. Skyrme-Hartree-Fock-Boguliubov and ab initio Gorkov-Green function calculations are challenged by the new measurements but reproduce qualitatively the observed shell effect.
A high-purity co-axial germanium detector has been calibrated in efficiency to a precision of about 0.15% over a wide energy range. High-precision scans of the detector crystal and gamma-ray source measurements have been compared to Monte-Carlo simul
ations to adjust the dimensions of a detector model. For this purpose, standard calibration sources and short-lived on-line sources have been used. The resulting efficiency calibration reaches the precision needed e.g. for branching ratio measurements of super-allowed beta decays for tests of the weak-interaction standard model.
