Phase transitions in superconducting mesoscopic disks have been studied over the H-T phase diagram through heat capacity measurement of an array of independent aluminium disks. These disks exhibit non periodic modulations versus H of the height of th
e heat capacity jump at the superconducting to normal transition. This behaviour is attributed to giant vortex states characterized by their vorticity L. A crossover from a bulk-like to a mesoscopic behaviour is demonstrated. $C_{rm p}$ versus H plots exhibit cascades of phase transitions as L increases or decreases by one unity, with a strong hysteresis. Phase diagrams of giant vortex states inside the superconducting region are drawn in the vortex penetration and expulsion regimes and phase transitions driven by temperature between vortex states are thus predicted in the zero field cooled regime before being experimentally evidenced.
The heat capacity $C_{p}$ of an array of independent aluminum rings has been measured under an external magnetic field $vec{H}$ using highly sensitive ac-calorimetry based on a silicon membrane sensor. Each superconducting vortex entrance induces a p
hase transition and a heat capacity jump and hence $C_{p}$ oscillates with $vec{H}$. This oscillatory and non-stationary behaviour measured versus the magnetic field has been studied using the Wigner-Ville distribution (a time-frequency representation). It is found that the periodicity of the heat capacity oscillations varies significantly with the magnetic field; the evolution of the period also depends on the sweeping direction of the field. This can be attributed to a different behavior between expulsion and penetration of vortices into the rings. A variation of more than 15% of the periodicity of the heat capacity jumps is observed as the magnetic field is varied. A description of this phenomenon is given using an analytical solution of the Ginzburg-Landau equations of superconductivity.
