Combined neutron and x-ray diffraction experiments demonstrate the formation of a low-temperature minority tetragonal phase in Ba$_{0.76}$K$_{0.24}$Fe$_2$As$_2$ in addition to the majority magnetic, orthorhombic phase. A coincident enhancement in the
magnetic ($frac{1}{2}$ $frac{1}{2}$ 1) peaks shows that this minority phase is of the same type that was observed in Ba$_{1-x}$Na$_x$Fe$_2$As$_2$ ($0.24 leq x leq 0.28$), in which the magnetic moments reorient along the $c$-axis. This is evidence that the tetragonal magnetic phase is a universal feature of the hole-doped iron-based superconductors.
We present neutron diffraction analysis of BaFe$_2$(As$_{1-x}$P$_x$)$_2$ over a wide temperature (10 to 300 K) and compositional ($0.11 leq x leq 0.79$) range, including the normal state, the magnetically ordered state, and the superconducting state.
The paramagnetic to spin-density wave and orthorhombic to tetragonal transitions are first order and coincident within the sensitivity of our measurements ($sim 0.5$ K). Extrapolation of the orthorhombic order parameter down to zero suggests that structural quantum criticality cannot exist at compositions higher than $x = 0.28$, which is much lower than values determined using other methods, but in good agreement with our observations of the actual phase stability range. The onset of spin-density wave order shows a stronger structural anomaly than the charge-doped system in the form of an enhancement of the $c/a$ ratio below the transition.
The upper critical fields, $H_{c2}$($T$), of single crystals of the superconductor Ca$_{10}$(Pt$_{4-delta}$As$_{8}$)((Fe$_{0.97}$Pt$_{0.03}$)$_{2}$As$_{2}$)$_{5}$ ($delta$ $approx$ 0.246) are determined over a wide range of temperatures down to $T$ =
1.42 K and magnetic fields of up to $mu_{0}H$ $simeq$ 92 T. The measurements of anisotropic $H_{c2}$($T$) curves are performed in pulsed magnetic fields using radio-frequency contactless penetration depth measurements for magnetic field applied both parallel and perpendicular to the textbf{ab}-plane. Whereas a clear upward curvature in $H_{c2}^{paralleltextbf{c}}$($T$) along textbf{H}$parallel$textbf{c} is observed with decreasing temperature, the $H_{c2}^{paralleltextbf{ab}}$($T$) along textbf{H}$parallel$textbf{ab} shows a flattening at low temperatures. The rapid increase of the $H_{c2}^{paralleltextbf{c}}$($T$) at low temperatures suggests that the superconductivity can be described by two dominating bands. The anisotropy parameter, $gamma_{H}$ $equiv$ $H_{c2}^{paralleltextbf{ab}}/H_{c2}^{paralleltextbf{c}}$, is $sim$7 close to $T_{c}$ and decreases considerably to $sim$1 with decreasing temperature, showing rather weak anisotropy at low temperatures.
