Subscribe to the gold package and get unlimited access to Shamra Academy
Register a new userCrystallographic reconstruction study of the effects of finish rolling temperature on the variant selection during bainite transformation in C-Mn high-strength steels
159
0
0.0
(
0
)
Ask ChatGPT about the research
No Arabic abstract
The effect of finish rolling temperature (FRT) on the austenite- () to-bainite () phase transformation is quantitatively investigated in high-strength C-Mn steels. In particular, the present study aims to clarify the respective contributions of the conditioning during the hot rolling and the variant selection (VS) during the phase transformation to the inherited texture. To this end, an alternative crystallographic reconstruction procedure, which can be directly applied to experimental electron backscatter diffraction (EBSD) mappings, is developed by combining the best features of the existing models: the orientation relationship (OR) refinement, the local pixel-by-pixel analysis and the nuclei identification and spreading strategy. The applicability of this method is demonstrated on both quenching and partitioning (Q&P) and as-quenched lath-martensite steels. The results obtained on the C-Mn steels confirm that the sample finish rolled at the lowest temperature (829{deg}C) exhibits the sharpest transformation texture. It is shown that this sharp texture is exclusively due to a strong VS from parent brass {110}<1-12>, S {213}<-3-64> and Goss {110}<001> grains, whereas the VS from the copper {112}<-1-11> grains is insensitive to the FRT. In addition, a statistical VS analysis proves that the habit planes of the selected variants do not systematically correspond to the predicted active slip planes using the Taylor model. In contrast, a correlation between the Bain group to which the selected variants belong and the FRT is clearly revealed, regardless of the parent orientation. These results are discussed in terms of polygranular accommodation mechanisms, especially in view of the observed development in the hot-rolled samples of high-angle grain boundaries with misorientation axes between <111> and <110> .
rate research
Read More
In the recent years graphitization of ion-beam induced amorphous layers became the basic tool for device fabrication in diamond. The etchable graphitic layers can be removed to form free-standing membranes into which the desired structures can be sculpted using FIB milling. The optical properties of the devices fabricated using this method are assumed on the model of sharp diamond-air interface. The real quality of this interface could depend on degree of graphitization of the amorphous damage layers after annealing. In the present work the graphitization process was studied using conventional and analytical TEM. It was found that annealing at 550 {deg}C results in a partial graphitization of the implanted volume with formation of the nano-crystalline graphitic phase sandwiched between layers of tetrahedral amorphous carbon. Annealing at 1400 {deg}C resulted in complete graphitization of the amorphous layers. The average size of graphite nano-crystals did not exceed 5 nm with predominant orientation of c-planes normal to the sample surface.
Tensile tests were conducted on dual-phase high-strength steel in a Split-Hopkinson Tension Bar at a strain-rate in the range of 150-600/s and in a servo-hydraulic testing machine at a strain-rate between 10-3 and 100/s. A novel specimen design was utilized for the Hopkinson bar tests of this sheet material. Digital image correlation was used together with high-speed photography to study strain localisation in the tensile specimens at high rates of strain. By using digital image correlation, it is possible to obtain in-plane displacement and strain fields during non-uniform deformation of the gauge section, and accordingly the strains associated with diffuse and localised necking may be determined. The full-field measurements in high strain-rate tests reveal that strain localisation started even before the maximum load was attained in the specimen. An elasto-viscoplastic constitutive model is used to predict the observed stress-strain behaviour and strain localisation for the dual-phase steel. Numerical simulations of dynamic tensile tests were performed using the non-linear explicit FE code LS-DYNA. Simulations were done with shell (plane stress) and brick elements. Good correlation between experiments and numerical predictions was achieved, in terms of engineering stress-strain behaviour, deformed geometry and strain fields. However, mesh density plays a role in the localisation of deformation in numerical simulations, particularly for the shell element analysis.
We have found that various Mn oxides have the universal resistivity and thermopower in the high temperature limit. The resistivities and thermopowers of all the samples go toward constant values of 7$pm$1 m$Omega$cm and $-79pm$3 $mu$V/K, which are independent of carrier density and crystal structures. We propose that the electric conduction occurs in a highly localized way in the high temperature limit, where the exchange of entropy and charge occurs in the neighboring Mn$^{3+}$ and Mn$^{4+}$ ions.
We study the effects of growth temperature, Ga:As ratio and post-growth annealing procedure on the Curie temperature, Tc, of (Ga,Mn)As layers grown by molecular beam epitaxy. We achieve the highest Tc values for growth temperatures very close to the 2D-3D phase boundary. The increase in Tc, due to the removal of interstitial Mn by post growth annealing, is counteracted by a second process which reduces Tc and which is more effective at higher annealing temperatures. Our results show that it is necessary to optimize the growth parameters and post growth annealing procedure to obtain the highest Tc.
It was recently reported that segregation of Zr to grain boundaries (GB) in nanocrystalline Cu can lead to the formation of disordered intergranular films [1,2]. In this study we employ atomistic computer simulations to study how the formation of these films affects the dislocation nucleation from the GBs. We found that full disorder of the grain boundary structure leads to the suppression of dislocation emission and significant increase of the yield stress. Depending on the solute concentration and heat-treatment, however, a partial disorder may also occur and this aids dislocation nucleation rather than suppressing it, resulting in elimination of the strengthening effect.
Log in to be able to interact and post comments
comments
Fetching comments
Sign in to be able to follow your search criteria
