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The Effect of Mechanical Cold Work on the Magnetic Flux Expulsion of Niobium

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 Added by Sam Posen
 Publication date 2018
  fields Physics
and research's language is English




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Expulsion of ambient flux has been shown to be crucial to obtain high quality factors in bulk niobium SRF cavities. However, there remain many questions as to what properties of the niobium material determine its flux expulsion behavior. In this paper, we present first results from a new study of two cavities that were specially fabricated to study flux expulsion. Both cavities were made from large grain ingot niobium slices, one of which had its slices rolled prior to fabrication, and none these slices were annealed prior to measurement. Expulsion measurements indicate that a dense network of grain boundaries is not necessary for a cavity to have near-complete flux trapping behavior up to large thermal gradients. The results also contribute to a body of evidence that cold work is a strong determinant of flux expulsion behavior in SRF-grade niobium.



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230 - S. Posen , G. Wu , E. Harms 2018
When a superconducting radiofrequency cavity is cooled through its critical temperature, ambient magnetic flux can become frozen in to the superconductor, resulting in degradation of the quality factor. This is especially problematic in applications where quality factor is a cost driver, such as in the CW linac for LCLS-II. Previously, it had been unknown how to prevent flux from being trapped during cooldown in bulk niobium cavities, but recent R&D studies showed near-full flux expulsion can be achieved through high temperature heat treatment and cooling cavities through the superconducting transition with a spatial thermal gradient over the surface. In this paper, we describe the first accelerator implementation of these procedures, in cryomodules that are currently being produced for LCLS-II. We compare the performance of cavities under different conditions of heat treatment and thermal gradient during cooldown, showing a substantial improvement in performance when both are applied, enabling cryomodules to reach and, in many cases, exceed a Q0 of ~3x10^10.
Even when cooled through its transition temperature in the presence of an external magnetic field, a superconductor can expel nearly all external magnetic flux. This Letter presents an experimental study to identify the parameters that most strongly influence flux trapping in high purity niobium during cooldown. This is critical to the operation of superconducting radiofrequency cavities, in which trapped flux degrades the quality factor and therefore cryogenic efficiency. Flux expulsion was measured on a large survey of 1.3 GHz cavities prepared in various ways. It is shown that both spatial thermal gradient and high temperature treatment are critical to expelling external magnetic fields, while surface treatment has minimal effect. For the first time, it is shown that a cavity can be converted from poor expulsion behavior to strong expulsion behavior after furnace treatment, resulting in a substantial improvement in quality factor. Future plans are described to build on this result in order to optimize treatment for future cavities.
Previous work has demonstrated that the radio frequency surface resistance of niobium resonators is dramatically reduced when nitrogen impurities are dissolved as interstitial in the material. The origin of this effect is attributed to the lowering of the Mattis and Bardeen surface resistance contribution with increasing accelerating field. Meanwhile, an enhancement of the sensitivity to trapped magnetic field is typically observed for such cavities. In this paper we conduct the first systematic study on these different components contributing to the total surface resistance as a function of different levels of dissolved nitrogen, in comparison with standard surface treatments for niobium resonators. Adding these results together we are able to show for the first time which is the optimum surface treatment that maximizes the Q-factor of superconducting niobium resonators as a function of expected trapped magnetic field in the cavity walls. These results also provide new insights on the physics behind the change in the field dependence of the Mattis and Bardeen surface resistance, and of the trapped magnetic vortex induced losses in superconducting niobium resonators.
106 - Bo Zhao 2011
Stars form in dense cores of magnetized molecular clouds. If the magnetic flux threading the cores is dragged into the stars, the stellar field would be orders of magnitude stronger than observed. This well-known magnetic flux problem demands that most of the core magnetic flux be decoupled from the matter that enters the star. We carry out the first exploration of what happens to the decoupled magnetic flux in 3D, using an MHD version of the ENZO adaptive mesh refinement code. The field-matter decoupling is achieved through a sink particle treatment, which is needed to follow the protostellar accretion phase of star formation. We find that the accumulation of the decoupled flux near the accreting protostar leads to a magnetic pressure buildup. The high pressure is released anisotropically, along the path of least resistance. It drives a low-density expanding region in which the decoupled magnetic flux is expelled. This decoupling-enabled magnetic structure has never been seen before in 3D MHD simulations of star formation. It generates a strong asymmetry in the protostellar accretion flow, potentially giving a kick to the star. In the presence of an initial core rotation, the structure presents an obstacle to the formation of a rotationally supported disk, in addition to magnetic braking, by acting as a rigid magnetic wall that prevents the rotating gas from completing a full orbit around the central object. We conclude that the decoupled magnetic flux from the stellar matter can strongly affect the protostellar collapse dynamics.
We report the rf performance of a single-cell superconducting radiofrequency cavity after low temperature baking in a nitrogen environment. A significant increase in quality factor has been observed when the cavity was heat treated in the temperature range of 120-160 {deg}C with a nitrogen partial pressure of ~25 mTorr. This increase in quality factor as well as the Q-rise phenomenon (anti-Q-slope) is similar to those previously obtained with high temperature nitrogen doping as well as titanium doping. In this study, a cavity N2-treated at 120 {deg}C and at140 {deg}C, showed no degradation in accelerating gradient, however the accelerating gradient was degraded by 25 with a 160 {deg}C N2 treatment. Sample coupons treated in the same conditions as the cavity were analyzed by scanning electron microscope, x-ray photoelectron spectroscopy and secondary ion mass spectroscopy revealed a complex surface composition of Nb_2O5, NbO and NbN(1-x)Ox within the rf penetration depth. Furthermore, magnetization measurements showed no significant change on bulk superconducting properties.
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