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Register a new userSuperconductivity with broken time reversal symmetry in ion irradiated Ba$_{0.27}$K$_{0.73}$Fe$_2$As$_2$ single crystals
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Over the last years a lot of theoretical and experimental efforts have been made to find states with broken time reversal symmetry (BTRS) in multi-band superconductors. In particular, it was theoretically proposed that in the Ba$_{1-x}$K$_{x}$Fe$_2$As$_2$ system either an $s+is$ or an $s+id$ BTRS state may exist at high doping levels in a narrow region of the phase diagram. Here we report the observation of an enhanced zero field muon spin relaxation rate below the superconducting transition temperature for a high quality crystalline sample with $x approx$ 0.73. This indicates that indeed the time reversal symmetry is broken in superconducting Ba$_{1-x}$K$_{x}$Fe$_2$As$_2$ at this doping level.
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Discoveries of ordered quantum states of matter are of great fundamental interest, and often lead to unique applications. The most well known example -- superconductivity -- is caused by the formation and condensation of pairs of electrons. A key property of superconductors is diamagnetism: magnetic fields are screened by dissipationless currents. Fundamentally, what distinguishes superconducting states from normal states is a spontaneously broken symmetry corresponding to long-range coherence of fermion pairs. Here we report a set of experimental observations in hole doped Ba$_{1-x}$K$_x$Fe$_2$As$_2$ which are not consistent with conventional superconducting behavior. Our specific-heat measurements indicate the formation of fermionic bound states when the temperature is lowered from the normal state. However, for $x sim 0.8$, instead of the standard for superconductors, zero resistance and diamagnetic screening, for a range of temperatures, we observe the opposite effect: the generation of self-induced magnetic fields measured by spontaneous Nernst effect and muon spin rotation experiments. The finite resistance and the lack of any detectable diamagnetic screening in this state exclude the spontaneously broken symmetry associated with superconducting two-fermion correlations. Instead, combined evidence from transport and thermodynamic measurements indicates that the formation of fermionic bound states leads to spontaneous breaking of time-reversal symmetry above the superconducting transition temperature. These results demonstrate the existence of a broken-time-reversal-symmetry bosonic metal state. In the framework of a multiband theory, such a state is characterized by quartic correlations: the long-range order exists only for {it pairs} of fermion pairs.
The noncentrosymmetric superconductor Re$_6$Zr has attracted much interest due to the observation of broken time-reversal symmetry in the superconducting state. Here we report an investigation of the superconducting gap structure of Re$_6$Zr single crystals by measuring the magnetic penetration depth shift $Deltalambda(T)$ and electronic specific heat $C_e(T)$. $Deltalambda(T)$ exhibits an exponential temperature dependence behavior for $T~ll~T_c$, which indicates a fully-open superconducting gap. Our analysis shows that a single gap $s$-wave model is sufficient to describe both the superfluid density $rho_s(T)$ and $C_e(T)$ results, with a fitted gap magnitude larger than the weak coupling BCS value, providing evidence for fully-gapped superconductivity in Re$_6$Zr with moderate coupling.
The temperature dependent resistivity of Ba$_{1-x}$K$_x$Fe$_2$As$_2$ (x = 0.23, 0.25, 0.28 and 0.4) single crystals and the angle dependent resistivity of superconducting Ba$_{0.6}$K$_{0.4}$Fe$_2$As$_2$ single crystals were measured in magnetic fields up to 9 T. The measurements of temperature dependent resistivity for samples with different doping levels revealed very high upper critical fields which increase with the transition temperature monotonously, and a very low superconducting anisotropy ratio $Gamma=H_{c2}^{ab}/H_{c2}^c approx$ 2. By scaling the resistivity in the frame of the anisotropic Ginzburg-Landau theory, the angle dependent resistivity of the Ba$_{0.6}$K$_{0.4}$Fe$_2$As$_2$ single crystal measured with different magnetic fields at a certain temperature collapsed onto one curve. As the only scaling parameter, the anisotropy $Gamma$ was determined alternatively for each temperature and was found to be between two and three.
A single crystal of isovalently substituted Ba(Fe$_{1-x}$Ru$_{x}$)$_2$As$_2$ ($x=0.24$) was sequentially irradiated with 2.5 MeV electrons up to a maximum dose of $2.1 times 10^{19}$ electrons/cm^2. The electrical resistivity was measured textit{in - situ} at $T=$22 K during the irradiation and textit{ex - situ} as a function of temperature between subsequent irradiation runs. Upon irradiation, the superconducting transition temperature, $T_c$, decreases and the residual resistivity, $rho_0$, increases. We find that electron irradiation leads to the fastest suppression of $T_c$ compared to other types of artificially introduced disorder, probably due to the strong short-range potential of the point-like irradiation defects. A more detailed analysis within a multiband scenario with variable scattering potential strength shows that the observed $T_c$ vs. $rho_0$ is fully compatible with $s_pm$ pairing, in contrast to earlier claims that this model leads to a too rapid a suppression of $T_c$ with scattering.
We report a detailed investigation on the lower critical field $H_{c1}$ of the superconducting Ba$_{0.6}$K$_{0.4}$Fe$_2$As$_2$ (FeAs-122) single crystals. A pronounced kink is observed on the $H_{c1}(T)$ curve, which is attributed to the existence of two superconducting gaps. By fitting the data $H_{c1}(T)$ to the two-gap BCS model in full temperature region, a small gap of $Delta_a(0)=2.0pm 0.3$ meV and a large gap of $Delta_b(0)=8.9pm 0.4$ meV are obtained. The in-plane penetration depth $lambda_{ab}(0)$ is estimated to be 105 nm corresponding to a rather large superfluid density, which points to the breakdown of the Uemura plot in FeAs-122 superconductors.
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