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Register a new userDry demagnetization cryostat for sub-millikelvin helium experiments: refrigeration and thermometry
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We demonstrate successful dry refrigeration of quantum fluids down to $T=0.16$,mK by using copper nuclear demagnetization stage that is pre-cooled by a pulse-tube-based dilution refrigerator. This type of refrigeration delivers a flexible and simple sub-mK solution to a variety of needs including experiments with superfluid $^3$He. Our central design principle was to eliminate relative vibrations between the high-field magnet and the nuclear refrigeration stage, which resulted in the minimum heat leak of $Q=4.4$,nW obtained in field of 35,mT. For thermometry, we employed a quartz tuning fork immersed into liquid $^3$He. We show that the fork oscillator can be considered as self-calibrating in superfluid $^3$He at the crossover point from hydrodynamic into ballistic quasiparticle regime.
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We report on microwave optomechanics measurements performed on a nuclear adiabatic demagnetization cryostat, whose temperature is determined by accurate thermometry from below 500$~mu$K to about 1$~$Kelvin. We describe a method for accessing the on-chip temperature, building on the blue-detuned parametric instability and a standard microwave setup. The capabilities and sensitivity of both the experimental arrangement and the developed technique are demonstrated with a very weakly coupled silicon-nitride doubly-clamped beam mode of about 4$~$MHz and a niobium on-chip cavity resonating around 6$~$GHz. We report on an unstable intrinsic driving force in the coupled microwave-mechanical system acting on the mechanics that appears below typically 100$~$mK. The origin of this phenomenon remains unknown, and deserves theoretical input. It prevents us from performing reliable experiments below typically 10-30$~$mK; however no evidence of thermal decoupling is observed, and we propose that the same features should be present in all devices sharing the microwave technology, at different levels of strengths. We further demonstrate empirically how most of the unstable feature can be annihilated, and speculate how the mechanism could be linked to atomic-scale two level systems. The described microwave/microkelvin facility is part of the EMP platform, and shall be used for further experiments within and below the millikelvin range.
The CUORE experiment is the worlds largest bolometric experiment. The detector consists of an array of 988 TeO2 crystals, for a total mass of 742 kg. CUORE is presently taking data at the Laboratori Nazionali del Gran Sasso, Italy, searching for the neutrinoless double beta decay of 130Te. A large custom cryogen-free cryostat allows reaching and maintaining a base temperature of about 10 mK, required for the optimal operation of the detector. This apparatus has been designed in order to achieve a low noise environment, with minimal contribution to the radioactive background for the experiment. In this paper, we present an overview of the CUORE cryostat, together with a description of all its sub-systems, focusing on the solutions identified to satisfy the stringent requirements. We briefly illustrate the various phases of the cryostat commissioning and highlight the relevant steps and milestones achieved each time. Finally, we describe the successful cooldown of CUORE.
We developed a cryogenic system on a rotating table that achieves sub-Kelvin conditions. The cryogenic system consists of a helium sorption cooler and a pulse tube cooler in a cryostat mounted on a rotating table. Two rotary-joint connectors for electricity and helium gas circulation enable the coolers to be operated and maintained with ease. We performed cool-down tests under a condition of continuous rotation at 20 rpm. We obtained a temperature of 0.23 K with a holding time of more than 24 hours, thus complying with catalog specifications. We monitored the systems performance for four weeks; two weeks with and without rotation. A few-percent difference in conditions was observed between these two states. Most applications can tolerate such a slight difference. The technology developed is useful for various scientific applications requiring sub-Kelvin conditions on rotating platforms.
We present the evaluation of two different design configurations of a two-stage PrNi$_5$ continuous nuclear demagnetization refrigerator. Serial and parallel configurations of the two stages are considered, with emphasis on the attainable cooling power at sub-mK temperatures and the impact of the design choices on the operation of the refrigerator. Numerical simulations of heat transfer in the setup are used to evaluate the performance of the refrigerator as well as the technological requirements for the essential thermal links. In accord with similar findings for adiabatic demagnetization refrigerators [Shirron, emph{Cryogenics} textbf{62}, 2014], our simulations show that the performance of both configurations improves as the thermal links improve, and that the parallel configuration yields a higher cooling power than the series design for a given thermal link resistance and sample temperature.
The National High Magnetic Field Laboratory (NHMFL) High B/T facility at the University of Florida in Gainesville provides a unique combination of ultra-low temperatures below 1 mK and high magnetic fields up to 16 T for user experiments. To meet the growing user demand for calorimetric and thermal transport measurements, particularly on milligram-sized solid samples, we are developing scaleable thermometers based on quartz tuning fork resonators immersed in liquid $^3$He. We demonstrate successful thermometer operation at the combined extreme conditions available at our user facility, and discuss the feasibility of fast and compact thermal probes.
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