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Register a new userUltrasonic monitoring of stress and cracks of the 1/3 scale mock-up of nuclear reactor concrete containment structure
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To evaluate the stress level and damage of a reinforced concrete containment wall and its reaction to pressure variations, we implemented successive ultrasonic experiments on the exterior surface of the containment wall in the gusset area for three consecutive years. During each experiment, the pressure inside the containment wall increased gradually from 0 MPa to 0.43 MPa and then decreased back to 0 Mpa.From the analysis of the ultrasonic coda waves obtained in the multiple scattering regime, we performed Coda Wave Interferometry to calculate the apparent velocity changes in the structure (denoted by $dV/V_a$) and Coda Wave Decorrelation (DC) measurements to produce 3D cartographies of stress and crack distribution. From three source-receiver pairs, located at the top, middle and bottom of the experimental region, we observe that coda waves dilate, shrink and remain almost unchanged, respectively. This corresponds to the decreasing, increasing and invariant pressure inside the concrete. The comparison of three years results demonstrates that the variation of $dV/V_a$ and DC under the same pressure test increases through the years, which indicates the progressive deterioration and aging of the concrete. From a large collection of source-receiver pairs at different times, the spatial-temporal variations of $dV/V_a$ and DC are then used to produce a map of the structural velocity and scattering changes, respectively. We observe a decreasing velocity on the top part and an increasing in the middle one, which is in line with the $dV/V_a$ analysis. The reconstructed scattering changes (or structural changes) highlight the active region during the inflation-deflation procedure, corresponding to the opening and closing (and sometimes the development) of cracks. The larger magnitude in 2019 than in 2017 indicates the increasing damage in the concrete.
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Microstructure characterization is of great value to understanding nuclear graphites properties and irradiation behavior. However, graphite is soft and could be easily damaged during sample preparation. A three-step polishing method involving mechanical polishing, ion milling and rapid oxidation is proposed for graphite. Ion milling is adopted to remove the broken graphite pieces produced by mechanical polishing. Rapid oxidation is then adopted to remove irradiation-induced damage layer during ion milling. The Raman spectra show very low G peak width and ID/IG ratio after rapid oxidation, indicating a surface completely free from artificial defects. The micro-cracks which were conventionally observed via a transmission electron microscope can be observed on rapid-oxidized surface in a scanning electron microscope. By digital image processing, the micro-cracks along with the gas-escape pores in nuclear graphite IG-110 are statistically analyzed. Porositys distributions on crack (pore) size (spanning from 10 nm to 100 um) are given, which could help to understand and simulate graphites performances in reactors.
Silicon carbide (SiC) is an excellent substrate for growth and manipulation of large scale, high quality epitaxial graphene. On the carbon face (the ($bar{1}bar{1}bar{1}$) or $(000bar{1}$) face, depending on the polytype), the onset of graphene growth is intertwined with the formation of several competing surface phases, among them a (3$times$3) precursor phase suspected to hinder the onset of controlled, near-equilibrium growth of graphene. Despite more than two decades of research, the precise atomic structure of this phase is still unclear. We present a new model of the (3$times$3)-SiC-($bar{1}bar{1}bar{1}$) reconstruction, derived from an {it ab initio} random structure search based on density functional theory including van der Waals effects. The structure consists of a simple pattern of five Si adatoms in bridging and on-top positions on an underlying, C-terminated substrate layer, leaving one C atom per (3$times$3) unit cell formally unsaturated. Simulated scanning tunneling microscopy (STM) images are in excellent agreement with previously reported experimental STM images.
In nature, barchan dunes typically exist as members of larger fields that display striking, enigmatic structures that cannot be readily explained by examining the dynamics at the scale of single dunes, or by appealing to patterns in external forcing. To explore the possibility that observed structures emerge spontaneously as a collective result of many dunes interacting with each other, we built a numerical model that treats barchans as discrete entities that interact with one another according to simplified rules derived from theoretical and numerical work and from field observations: (1) Dunes exchange sand through the fluxes that leak from the downwind side of each dune and are captured on their upstream sides; (2) when dunes become sufficiently large, small dunes are born on their downwind sides (`calving); and (3) when dunes collide directly enough, they merge. Results show that these relatively simple interactions provide potential explanations for a range of field-scale phenomena including isolated patches of dunes and heterogeneous arrangements of similarly sized dunes in denser fields. The results also suggest that (1) dune field characteristics depend on the sand flux fed into the upwind boundary, although (2) moving downwind, the system approaches a common attracting state in which the memory of the upwind conditions vanishes. This work supports the hypothesis that calving exerts a first-order control on field-scale phenomena; it prevents individual dunes from growing without bound, as single-dune analyses suggest, and allows the formation of roughly realistic, persistent dune field patterns.
The stability, structure and properties of carbonate minerals at lower mantle conditions has significant impact on our understanding of the global carbon cycle and the composition of the interior of the Earth. In recent years, there has been significant interest in the behavior of carbonates at lower mantle conditions, specifically in their carbon hybridization, which has relevance for the storage of carbon within the deep mantle. Using high-pressure synchrotron X-ray diffraction in a diamond anvil cell coupled with direct laser heating of CaCO$_{3}$ using a CO$_{2}$ laser, we identify a crystalline phase of the material above 40 GPa $-$ corresponding to a lower mantle depth of around 1,000 km $-$ which has first been predicted by textit{ab initio} structure predictions. The observed $sp^{2}$ carbon hybridized species at 40 GPa is monoclinic with $P2_{1}/c$ symmetry and is stable up to 50 GPa, above which it transforms into a structure which cannot be indexed by existing known phases. A combination of textit{ab initio} random structure search (AIRSS) and quasi-harmonic approximation (QHA) calculations are used to re-explore the relative phase stabilities of the rich phase diagram of CaCO$_{3}$. Nudged elastic band (NEB) calculations are used to investigate the reaction mechanisms between relevant crystal phases of CaCO$_{3}$ and we postulate that the mineral is capable of undergoing $sp^{2}$-$sp^{3}$ hybridization change purely in the $P2_{1}/c$ structure $-$ forgoing the accepted post-aragonite $Pmmn$ structure.
The Weyl semimetal NbP exhibits a very small Fermi surface consisting of two electron and two hole pockets, whose fourfold degeneracy in $k$ space is tied to the rotational symmetry of the underlying tetragonal crystal lattice. By applying uniaxial stress, the crystal symmetry can be reduced, which successively leads to a degeneracy lifting of the Fermi-surface pockets. This is reflected by a splitting of the Shubnikov-de Haas frequencies when the magnetic field is aligned along the $c$ axis of the tetragonal lattice. In this study, we present the measurement of Shubnikov-de Haas oscillations of single-crystalline NbP samples under uniaxial tension, combined with state-of-the-art calculations of the electronic band structure. Our results show qualitative agreement between calculated and experimentally determined Shubnikov-de Haas frequencies, demonstrating the robustness of the band-structure calculations upon introducing strain. Furthermore, we predict a significant shift of the Weyl points with increasing uniaxial tension, allowing for an effective tuning to the Fermi level at only 0.8% of strain along the $a$ axis.
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