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Register a new userMethods to simplify cooling of liquid Helium cryostats
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Liquid Helium is used widely, from hospitals to characterization of materials at low temperatures. Many experiments at low temperatures require liquid Helium, particularly when vibration isolation precludes the use of cryocoolers and when one needs to cool heavy equipment such as superconducting coils. Here we describe methods to simplify the operations required to use liquid Helium by eliminating the use of high pressure bottles, avoiding blockage and improving heating and cooling rates. First we show a simple and very low cost method to transfer liquid Helium from a transport container into a cryostat that uses a manual pump having pumping and pressurizing ports, giving a liquid Helium transfer rate of about 100 liters an hour. Second, we describe a closed cycle circuit of Helium gas cooled in an external liquid nitrogen bath that allows precooling a cryogenic experiment without inserting liquid nitrogen into the cryostat, eliminating problems associated to the presence of nitrogen around superconducting magnets. And third, we show a sliding seal assembly and an inner vacuum chamber design that allows inserting large experiments into liquid Helium.
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We introduce a scattering-type scanning near-field infrared microscope (s-SNIM) for the local scale near- field sample analysis and spectroscopy from room (RT) down to liquid helium (LHe) temperatures. The extension of s-SNIM down to T = 5K is in particular crucial for low-temperature phase transitions, e.g. for the examination of superconductors, as well as low energy excitations. The LT s-SNIM performance is tested with CO2-IR excitation at T = 7K using a bare Au reference and a structured Si/SiO$_2$-sample. Furthermore, we quantify the impact of local laser heating under the s-SNIM tip apex by monitoring the light-induced ferroelectric-to-paraelectric phase transition of the skyrmion-hosting multiferroic material GaV4S8 at T$_c$ = 42K. We apply LT s-SNIM to study the spectral response of GaV$_4$S$_8$ and its lateral domain structure in the ferroelectric phase by the mid-IR to THz free-electron laser-light source FELBE at the Helmholtz-Zentrum Dresden-Rossendorf, Germany. Notably, our s-SNIM is based on a non-contact atomic force microscope(AFM), and thus can be complemented in-situ by various other AFM techniques, such as topography profiling, piezo-response force microscopy (PFM) and/or Kelvin-probe force microscopy (KPFM). The combination of these methods support the comprehensive study of the mutual interplay in the topographic, electronic and optical properties of surfaces from room temperature down to 5K.
Helium has the lowest boiling point of any element in nature at normal atmospheric pressure. Therefore, any unwanted substance like impurities present in liquid helium will be frozen and will be in solid form. Even if these solid impurities can be easily eliminated by filtering, liquid helium may contain a non-negligible quantity of molecular hydrogen. These traces of molecular hydrogen are the causes of a known problem worldwide: the blocking of fine-capillary tubes used as flow impedances in helium evaporation cryostats to achieve temperatures below 4,2K. This problem seriously affects a wide range of cryogenic equipment used in low-temperature physics research and leads to a dramatic loss of time and costs due to the high price of helium. Here, we present first the measurement of molecular hydrogen content in helium gas. Three measures to decrease this molecular hydrogen are afterward proposed; (i) improving the helium quality, (ii) release of helium gas in the atmosphere during purge time for the regeneration cycle of the helium liquefiers internal purifier, and (iii) installation of two catalytic converters in a closed helium circuit. These actions have eliminated our low-temperature impedance blockage occurrences now for more than two years.
Pulse-tube based dilution refrigerators are massively employed in low temperature physics. They allow to reduce the running costs and to be operated with unprecedented easiness. However, the main drawback of this technology is the mechanical vibrations induced by the pulse-tube cryocooler. These perturbations can cause extra-noises drastically affecting the detector performance. In this paper, we propose a solution to mitigate the impact of these vibrations by mounting the detectors in an elastic-pendulum based suspended tower. Based on vibration modeling and experimental tests, we show that the vibration levels are attenuated by up to two orders of magnitude at most frequencies, especially above $sim20$ Hz, for both vertical and radial directions. Thanks to this passive isolation solution, vibration levels, both along vertical and radial directions, below 1 $mutextrm{g/}sqrt{text{Hz}}$ in the frequency range [1-1000] Hz are obtained. This provides a convenient environment to test the ultimate performance of low temperature detectors. As a result, we report an improvement by one to two orders of magnitude on the noise levels of massive cryogenic bolometers, leading to thermal energy resolutions improved by a factor 5 to 40. Finally, we conclude that the energy resolution of our cryogenic bolometers are no longer limited from any residual vibrations, hence allowing the perspective of further improving our bolometer performance in the context of low-mass dark matter searches and neutrino physics applications.
We report on the evaluation of microwave frequency synthesis using two cryogenic sapphire oscillators developed at the University of Western Australia. A down converter is used to make comparisons between microwave clocks at different frequencies, where the synthesized signal has a stability not significantly different from the reference oscillator. By combining the CSO with a H-maser, a reference source of arbitrary frequency at X-band can be synthesized with a fractional frequency stability of sub-$4 times 10^{-15}$ for integration times between 1 s and 10,000 s.
The dependence on applied electric field ($0 - 40$ kV/cm) of the scintillation light produced by fast electrons and $alpha$ particles stopped in liquid helium in the temperature range of 0.44 K to 3.12 K is reported. For both types of particles, the reduction in the intensity of the scintillation signal due to the applied field exhibits an apparent temperature dependence. Using an approximate solution of the Debye-Smoluchowski equation, we show that the apparent temperature dependence for electrons can be explained by the time required for geminate pairs to recombine relative to the detector signal integration time. This finding indicates that the spatial distribution of secondary electrons with respect to their geminate partners possesses a heavy, non-Gaussian tail at larger separations, and has a dependence on the energy of the primary ionization electron. We discuss the potential application of this result to pulse shape analysis for particle detection and discrimination.
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