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Register a new userUpper and lower critical fields in NdFeAs(O,F) single crystals : a study by Hall probe magnetization and specific heat
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The upper and lower critical fields have been deduced from specific heat and Hall probe magnetization measurements in non-optimally doped NdFeAs(O,F) single crystals ($T_c sim 32-35$K). The anisoptropy of the penetration depth ($Gamma_lambda$) is temperature independent and on the order of $4.0 pm 1.5$. Similarly specific heat data lead an anisotropy of the coherence lenght $Gamma_xi sim 5.5 pm 1.5$ close to $T_c$. Our results suggest the presence of rather large thermal fluctuations and to the existence of a vortex liquid phase over a broad temperature range ($sim 5$K large at 2T).
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Through a direct comparison of specific heat and magneto-resistance we critically asses the nature of superconducting fluctuations in the same nano-gram crystal of SmFeAs(O, F). We show that although the superconducting fluctuation contribution to conductivity scales well within the 2D-LLL scheme its predictions contrast the inherently 3D nature of SmFeAs(O, F) in the vicinity T_{c}. Furthermore the transition seen in specific heat cannot be satisfactory described either by the LLL or the XY scaling. Additionally we have validated, through comparing Hc2 values obtained from the entropy conservation construction (Hab=-19.5 T/K and Hab=-2.9 T/K), the analysis of fluctuation contribution to conductivity as a reasonable method for estimating the Hc2 slope.
Superconductivity of Ca1-xLaxFe2As2 single crystals with various doping level were investigated via electromagnetic measurements for out-plane (H//c) and in-plane (H//ab) directions. Obvious double superconducting transitions, which can survive in magnetic fields up to several Tesla, were observed in the medium-doped (x = 0.13) sample. Two kinds of distinct Hc2 phase diagrams were established for the low superconducting phase with Tc lower than 15 K and the high superconducting phase with Tc of over 40 K, respectively. Both the two kinds of phase diagrams exist in the medium-doped sample. Unusual upward curvature near Tc was observed in Hc2 phase diagrams and analyzed in detail. Temperature dependences of anisotropy for different doping concentrations were obtained and compared. Both superconducting phases manifest extremely large anisotropies, which may originate from the interface or intercalation superconductivity.
The H-T phase diagrams of single crystalline electron-doped K0.83Fe1.83Se2 (KFS1), K0.8Fe2Se2 (KFS2) and hole-doped Eu0.5K0.5Fe2As2 (EKFA) have been deduced from tunnel diode oscillator-based contactless measurements in pulsed magnetic fields up to 57 T for the inter-plane (H//c) and in-plane (H//ab) directions. The temperature dependence of the upper critical magnetic field Hc2(T) relevant to EFKA is accounted for by the Pauli model including an anisotropic Pauli paramagnetic contribution (mu_BHp=114 T for H//ab and 86 T for H//c). This is also the case of KFS1 and KFS2 for H//ab whereas a significant upward curvature, accounted for by a two-gap model, is observed for H//c. Despite the presence of antiferromagnetic lattice order within the superconducting state of the studied compounds, no influence of magnetic ordering on the temperature dependence of Hc2(T) is observed.
Optimally-doped La1.85Sr0.15CuO4 single crystals have been investigated by dc and ac magnetic measurements. These crystals have rectangular needle-like shapes with the long needle axis parallel to the crystallographic c axis (c-crystal) or parallel to the basal planes (a-crystal). In both crystals, the temperature dependence of the upper critical fields (HC2) and the surface critical field (HC3) were measured. The H-T phase diagram is presented. Close to TC =35 K, for the c-crystal, {gamma}c = / = 1.80(2), whereas for the a-crystal the {gamma}a = / =4.0(2) obtained, is much higher than the theoretical value 1.69. At low applied dc fields, positive field-cooled branches known as the paramagnetic Meissner effect (PME) are observed, their magnitude is inversely proportional to H. The anisotropic PME is observed in both a- and c-crystals, only when the applied field is along the basal planes. It is speculated that the high {gamma}a and the PME are connected to each other.
We present heat capacity measurements of the upper critical fields of single-crystal NdFeAsO1-xFx. In zero-magnetic field a clear step in the heat capacity is observed at Tc = 47K . In fields applied perpendicular to the FeAs-layers the step broadens significantly whereas for the in-plane orientation the field effects are small. This behavior is reminiscent of the CuO2-high-Tc superconductors and is a manifestation of pronounced fluctuation effects. Using an entropy conserving construction we determine the transition temperatures in applied fields and the upper critical field slopes of dHc2,a = -0.72 T/K and dHc2,ab = -3.1 T/K. Zero-temperature coherence lengths of xiab = 3.7 nm and xic = 0.9 nm and a modest superconducting anisotropy of gamma ~ 4 can be deduced in a single-band model.
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