The objective of this study is to study some of the optimal analytical conditions for the
determination of the Cu2+ ion using potentiometric titration method using the platinum
electrode as a working electrode and the AgCL/Ag as a Reference electro
de.
In this study, the technical conditions were studied (working Electrode type, Reference
Electrode type, Direction of titration, delay time, Proportional band, Speed of stirring)
and the analytical conditions (pH value, time factor, quantity of solid KI added, electrolyte
type and its concentration, detection limit) were studied using oxidation - reduction
reactions as the method of iodide titration which applied successfully electrochemical for
determine the Cu2+ ion.
Quality Control procedure Of Gamma Spectrometry measurements using
semi conductor HPGe Detectors and determination the uncertainty budget of
the measurements and calibrations have been prepared.
Depending on this procedure we can evaluate the qual
ity of the results to be
accepted or not, and where the correction actions should be used.