We report a measurement of the spin-flip probabilities for ultracold neutrons interacting with surfaces coated with nickel phosphorus. For 50~$mu$m thick nickel phosphorus coated on stainless steel, the spin-flip probability per bounce was found to be $beta_{rm NiP;on;SS} = (3.3^{+1.8}_{-5.6}) times 10^{-6}$. For 50~$mu$m thick nickel phosphorus coated on aluminum, the spin-flip probability per bounce was found to be $beta_{rm NiP;on;Al} = (3.6^{+2.1}_{-5.9}) times 10^{-6}$. For the copper guide used as reference, the spin flip probability per bounce was found to be $beta_{rm Cu} = (6.7^{+5.0}_{-2.5}) times 10^{-6}$. The results on the nickel phosphorus-coated surfaces may be interpreted as upper limits, yielding $beta_{rm NiP;on;SS} < 6.2 times 10^{-6}$ (90% C.L.) and $beta_{rm NiP;on;Al} < 7.0 times 10^{-6}$ (90% C.L.) for 50~$mu$m thick nickel phosphorus coated on stainless steel and 50~$mu$m thick nickel phosphorus coated on aluminum, respectively. Nickel phosphorus coated stainless steel or aluminum provides a solution when low-cost, mechanically robust, and non-depolarizing UCN guides with a high-Fermi-potential are needed.
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