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Possible Evidence for A Slush Vortex Phase in the Vicinity of Vortex Glass Transition in YBa$_{2}$Cu$_3$O$_{7-delta}$ Thin Films

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 Added by Shiliang Li
 Publication date 2001
  fields Physics
and research's language is English




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Current-voltage $I-V$ curves have been carefully measured for YBa$_2$Cu$_3$O$_{7-delta}$ thin films by following different thermal or field annealing procedures. Although all data can be described quite well by the vortex-glass theory, it is found that the dissipation in a small region just above the vortex-glass transition is history dependent: the dissipation in the warming up or field-increasing process is larger than that in the cooling down or field-decreasing process. We attribute this history dependent dissipation to possible existence of a slush vortex phase.



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We investigate the effect of the anisotropy and of the directional pinning in YBa$_2$Cu$_3$O$_{7-x}$ films grown by pulsed laser ablation from targets containing BaZrO$_3$ at 5% mol. BaZrO$_3$ inclusions self-assemble to give nanorods oriented along the c-axis, thus giving a preferential direction for vortex pinning. The directionality of vortex response is studied at high ac frequency with the complex microwave response at 48 GHz, as a function of the applied field and of the angle $theta$ between the field and the c-axis. The complex microwave response does not exhibit any angular scaling, suggesting that the structural anisotropy of YBa$_2$Cu$_3$O$_{7-x}$ is supplemented by at least another preferred orientation. The pinning parameter $r$ shows evidence of directional pinning, effective in a wide range of angles around the c-axis (thus ascribed to BZO nanocolumns).
100 - B. Maiorov , E. Osquiguil 2001
We report on the scaling of transport properties around the vortex melting in YBa$_2$Cu$_3$O$_{7- delta}$ oriented-twin single crystals in applied magnetic fields between 1T and 18T. We find that for all the measured field range the linear resistivity scales as $rho (t,theta) sim t^{sy} {cal F}_{pm} (sin(theta)t^{-sx})$, with $t=|T-T_{BG}|$ and $theta$ the angle between de planar defects and the magnetic field. The scaling is valid only for angles where the transition temperature $T_{BG} (theta)$ shows a cusp. The critical exponents $sx$ and $sy$ are in agreement with the values predicted by Lidmar and Wallin only at magnetic fields below 4T. A change in the value of $sx$ from $sx = 1 pm 0.2$ to $sx = 3 pm 0.2$ at around $H^{cr} approx $ 4T when the magnetic field is increased, is responsible for changes in the shape of the $T_{BG} (theta)$ curve and in the dependence of the linear dissipation on temperature and angle. The results strongly suggest the existence of a different vortex glassy phase in twinned crystals compared to the Bose-glass state found in samples with linear defects.
Most measurements of critical current densities in YBa$_2$Cu$_3$O$_{7-delta}$ thin films to date have been performed on films where the textit{c}-axis is grown normal to the film surface. With such films, the analysis of the dependence of $j_c$ on the magnetic field angle is complex. The effects of extrinsic contributions to the angular field dependence of $j_c$, such as the measurement geometry and disposition of pinning centres, are convoluted with those intrinsically due to the anisotropy of the material. As a consequence of this, it is difficult to distinguish between proposed FLL structure models on the basis of angular critical current density measurements on textit{c}-axis films. Films grown on mis-cut (vicinal) substrates have a reduced measurement symmetry and thus provide a greater insight into the critical current anisotropy. In this paper previous descriptions of the magnetic field angle dependence of $j_c$ in YBa$_2$Cu$_3$O$_{7-delta}$ are reviewed. Measurements on YBa$_2$Cu$_3$O$_{7-delta}$ thin films grown on a range of vicinal substrates are presented and the results interpreted in terms of the structure and dimensionality of the FLL in YBa$_2$Cu$_3$O$_{7-delta}$. There is strong evidence for a transition in the structure of the flux line lattice depending on magnetic field magnitude, orientation and temperature. As a consequence, a simple scaling law can not, by itself, describe the observed critical current anisotropy in YBa$_2$Cu$_3$O$_{7-delta}$. The experimentally obtained $j_c(theta)$ behaviour of YBCO is successfully described in terms of a kinked vortex structure for fields applied near parallel to the textit{a-b} planes.
We have grown and characterized 30 nm thick YBa$_2$Cu$_3$O$_{7-delta}$ (YBCO) films, deposited by pulsed laser deposition on both MgO (110) and SrTiO$_3$ (001) substrates, which induce opposite strain to the superconducting layer. By carefully tuning the in-situ post-annealing oxygen pressure, we achieved, in a reproducible way, films at different oxygen doping, spanning from the slightly overdoped down to the strongly underdoped region of the phase diagram. The transport properties of the films, investigated through resistance versus temperature measurements, are in perfect qualitative agreement with single crystals. Starting from these films, we have also successfully fabricated nanowires with widths down to 65 nm, at different oxygen doping. The nanostructures exhibit characteristic temperatures (as the critical temperature $T_{mathrm{c}}$ and the pseudogap temperature $T^*$) similar to those of the as-grown films and carry critical current densities $J_{mathrm{c}}$ close to the critical depairing value, limited by vortex entry. This implies that the superconducting and the normal state properties of underdoped YBCO are preserved in our films, and they can be studied as a function of the dimensionality of the system, down to the nanoscale.
We used a micromechanical torsional oscillator to measure the magnetic response of a twinned YBa$_2$Cu$_3$O$_{7-delta}$ single crystal disk near the Bose glass transition. We observe an anomaly in the temperature dependence of the magnetization consistent with the appearance of a magnetic shielding perpendicular to the correlated pinning of the twin boundaries. This effect is related to the thermodynamic transition from the vortex liquid phase to a Bose glass state.
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