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Register a new userSub-100 nanosecond temporally resolved imaging with the Medipix3 direct electron detector
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Detector developments are currently enabling new capabilities in the field of transmission electron microscopy (TEM). We have investigated the limits of a hybrid pixel detector, Medipix3, to record dynamic, time varying, electron signals. Operating with an energy of 60keV, we have utilised electrostatic deflection to oscillate electron beam position on the detector. Adopting a pump-probe imaging strategy we have demonstrated that temporal resolutions three orders of magnitude smaller than are available for typically used TEM imaging detectors are possible. Our experiments have shown that energy deposition of the primary electrons in the hybrid pixel detector limits the overall temporal resolution. Through adjustment of user specifiable thresholds or the use of charge summing mode, we have obtained images composed from summing 10,000s frames containing single electron events to achieve temporal resolution less than 100ns. We propose that this capability can be directly applied to studying repeatable material dynamic processes but also to implement low-dose imaging schemes in scanning transmission electron microscopy.
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Hybrid pixel sensor technology such as the Medipix3 represents a unique tool for electron imaging. We have investigated its performance as a direct imaging detector using a Transmission Electron Microscope (TEM) which incorporated a Medipix3 detector with a 300 micrometre thick silicon layer compromising of 256x256 pixels at 55 micrometre pixel pitch. We present results taken with the Medipix3 in Single Pixel Mode (SPM) with electron beam energies in the range, 60 to 200 keV. Measurements of the Modulation Transfer Function (MTF) and the Detective Quantum Efficiency (DQE) were investigated. At a given beam energy, the MTF data was acquired by deploying the established knife edge technique. Similarly, the experimental data required to DQE was obtained by acquiring a stack of images of a focused beam and of free space (flatfield) to determine the Noise Power Spectrum (NPS).
We have developed a prototype time-resolved neutron imaging detector employing a micro-pattern gaseous detector known as the micro-pixel chamber ({mu}PIC) coupled with a field-programmable-gate-array-based data acquisition system. Our detector system combines 100{mu}m-level spatial and sub-{mu}s time resolutions with a low gamma sensitivity of less than 10^-12 and high data rates, making it well suited for applications in neutron radiography at high-intensity, pulsed neutron sources. In the present paper, we introduce the detector system and present several test measurements performed at NOBORU (BL10), J-PARC to demonstrate the capabilities of our prototype. We also discuss future improvements to the spatial resolution and rate performance.
We developed a new sub-nanosecond time-resolved instrument to study the dynamics of UV-visible luminescence under high stopping power heavy ion irradiation. We applied our instrument, called SPORT, on a fast plastic scintillator (BC-400) irradiated with 27-MeV Ar ions having high mean electronic stopping power of 2.6 MeV/mu m. As a consequence of increasing permanent radiation damages with increasing ion fluence, our investigations reveal a degradation of scintillation intensity together with, thanks to the time-resolved measurement, a decrease in the decay constant of the scintillator. This combination indicates that luminescence degradation processes by both dynamic and static quenching, the latter mechanism being predominant. Under such high density excitation, the scintillation deterioration of BC-400 is significantly enhanced compared to that observed in previous investigations, mainly performed using light ions. The observed non-linear behaviour implies that the dose at which luminescence starts deteriorating is not independent on particles stopping power, thus illustrating that the radiation hardness of plastic scintillators can be strongly weakened under high excitation density in heavy ion environments.
We have developed a prototype time-resolved neutron imaging detector employing the micro-pixel chamber (muPIC), a micro-pattern gaseous detector, coupled with a field programmable gate array-based data acquisition system for applications in neutron radiography at high-intensity neutron sources. The prototype system, with an active area of 10cm x 10cm and operated at a gas pressure of 2 atm, measures both the energy deposition (via time-over-threshold) and 3-dimensional track of each neutron-induced event, allowing the reconstruction of the neutron interaction point with improved accuracy. Using a simple position reconstruction algorithm, a spatial resolution of 349 +/- 36 microns was achieved, with further improvement expected. The detailed tracking allows strong rejection of background gamma-rays, resulting in an effective gamma sensitivity of 10^-12 or less, coupled with stable, robust neutron identification. The detector also features a time resolution of 0.6 microseconds.
We present a detailed study of the spatial resolution of our time-resolved neutron imaging detector utilizing a new neutron position reconstruction method that improves both spatial resolution and event reconstruction efficiency. Our prototype detector system, employing a micro-pattern gaseous detector known as the micro-pixel chamber ({mu}PIC) coupled with a field-programmable-gate-array-based data acquisition system, combines 100{mu}m-level spatial and sub-{mu}s time resolutions with excellent gamma rejection and high data rates, making it well suited for applications in neutron radiography at high-intensity, pulsed neutron sources. From data taken at the Materials and Life Science Experimental Facility within the Japan Proton Accelerator Research Complex (J-PARC), the spatial resolution was found to be approximately Gaussian with a sigma of 103.48 +/- 0.77 {mu}m (after correcting for beam divergence). This is a significant improvement over that achievable with our previous reconstruction method (334 +/- 13 {mu}m), and compares well with conventional neutron imaging detectors and with other high-rate detectors currently under development. Further, a detector simulation indicates that a spatial resolution of less than 60 {mu}m may be possible with optimization of the gas characteristics and {mu}PIC structure. We also present an example of imaging combined with neutron resonance absorption spectroscopy.
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