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Register a new userFabrication and Characterization of an Amperometric Glucose Sensor on a Flexible Polyimide Substrate
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This study details the use of printing and other additive processes to fabricate a novel amperometric glucose sensor. The sensor was fabricated using a Au coated 12.7 micron polyimide film as a starting material, where micro-contact printing, electrochemical plating and chloridization, electrohydrodynamic jet (e-jet) printing, and spin coating were used to pattern, deposit, print, and coat functional materials, respectively. We have found that e-jet printing was effective for the deposition and patterning of glucose oxidase inks between ~5 to 1000 micron in width, and we have demonstrated that the enzyme was still active after printing. The thickness of the permselective layer was optimized to obtain a linear response to glucose concentration up to 32 mM. For these sensors no response to acetaminophen, a common interfering compound, was observed.
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We have fabricated resonant terahertz metamaterials on free standing polyimide substrates. The low-loss polyimide substrates can be as thin as 5.5 micron yielding robust large-area metamaterials which are easily wrapped into cylinders with a radius of a few millimeters. Our results provide a path forward for creating multi-layer non-planar metamaterials at terahertz frequencies.
We report a scalable approach to synthesize a large-area (up to 4 mm) thin black phosphorus (BP) film on a flexible substrate. We first deposited a red phosphorus (RP) thin-film on a flexible polyester substrate, followed by its conversion to BP in a high-pressure multi-anvil cell at room temperature. Raman spectroscopy and transmission electron microscopy measurements confirmed the formation of a nano-crystalline BP thin-film with a thickness of around 40 nm. Optical characterization indicates a bandgap of around 0.28 eV in the converted BP, similar to the bandgap measured in exfoliated thin-films. Thin-film BP transistors exhibit a field-effect mobility of around 0.5 cm2/Vs, which can probably be further enhanced by the optimization of the conversion process at elevated temperatures. Our work opens the avenue for the future demonstration of large-scale, high quality thin-film black phosphorus.
Flexible magnetic devices, i.e., magnetic devices fabricated on flexible substrates, are very attractive in application of detecting magnetic field in arbitrary surface, non-contact actuators, and microwave devices due to the stretchable, biocompatible, light-weight, portable, and low cost properties. Flexible magnetic films are essential for the realization of various functionalities of flexible magnetic devices. To give a comprehensive understanding for flexible magnetic films and related devices, we have reviewed recent advances in the studies of flexible magnetic films including fabrication methods, magnetic and transport properties of flexible magnetic films, and their applications in magnetic sensors, actuators, and microwave devices. Three typical methods were introduced to prepare the flexible magnetic films. Stretching or bending the flexible magnetic films offers a good way to apply mechanical strain on magnetic films, so that magnetic anisotropy, exchanged bias, coercivity, and magnetoresistance can be effectively manipulated. Finally, a series of examples were shown to demonstrate the great potential of flexible magnetic films for future applications.
The demand of fast and power efficient spintronics devices with flexibility requires additional energy for magnetization manipulation. Stress/and strain have shown their potentials for tuning magnetic properties to the desired level. Here, we report a systematic study for the effect of both tensile and compressive stresses on the magnetic anisotropy (MA). Further the effect of stress on the domain structure and magnetization relaxation mechanism in a perpendicularly magnetized Co/Pt film has been studied. It is observed that a minimal in-plane tensile strain has increased the coercivity of the film by 38$%$ of its initial value, while a very small change of coercivity has been found under compressive strain. The size of ferromagnetic domains decreases under tensile strain, while no change is observed under the compressive strain. Magnetization relxation measured at sub-coercive fields yields longer relaxation time in the strained state.
This paper reports the synthesis and detailed characterization of graphite thin films produced by thermal decomposition of the (0001) face of a 6H-SiC wafer, demonstrating the successful growth of single crystalline films down to approximately one graphene layer. The growth and characterization were carried out in ultrahigh vacuum (UHV) conditions. The growth process and sample quality were monitored by low-energy electron diffraction, and the thickness of the sample was determined by core level x-ray photoelectron spectroscopy. High-resolution angle-resolved photoemission spectroscopy shows constant energy map patterns, which are very sharp and fully momentum-resolved, but nonetheless not resolution limited. We discuss the implications of this observation in connection with scanning electron microscopy data, as well as with previous studies.
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