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Register a new userHigh-resolution kaonic-atom x-ray spectroscopy with transition-edge-sensor microcalorimeters
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We are preparing for an ultra-high resolution x-ray spectroscopy of kaonic atoms using an x-ray spectrometer based on an array of superconducting transition-edge-sensor microcalorimeters developed by NIST. The instrument has excellent energy resolutions of 2 - 3 eV (FWHM) at 6 keV and a large collecting area of about 20 mm^2. This will open new door to investigate kaon-nucleus strong interaction and provide new accurate charged-kaon mass value.
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High-resolution pionic-atom x-ray spectroscopy was performed with an x-ray spectrometer based on a 240-pixel array of superconducting transition-edge-sensor (TES) microcalorimeters at the piM1 beam line of the Paul Scherrer Institute. X-rays emitted by pionic carbon via the 4f->3d transition and the parallel 4d->3p transition were observed with a full-width-at-half-maximum energy resolution of 6.8 eV at 6.4 keV. Measured x-ray energies are consistent with calculated electromagnetic values which considered the strong-interaction effect assessed via the Seki-Masutani potential for the 3p energy level, and favor the electronic population of two filled 1s electrons in the K-shell. Absolute energy calibration with an uncertainty of 0.1 eV was demonstrated under a high-rate hadron beam condition of 1.45 MHz. This is the first application of a TES spectrometer to hadronic-atom x-ray spectroscopy and is an important milestone towards next-generation high-resolution kaonic-atom x-ray spectroscopy.
The Transition-Edge Sensor (TES) is an extremely sensitive device which is used to measure the energy of individual X-ray photons. For astronomical spectrometry applications, SRON develops a Frequency Domain Multiplexing (FDM) read-out system for kilopixel arrays of such TESs. Each TES is voltage biased at a specific frequency in the range 1 to 5 MHz. Isolation between the individual pixels is obtained through very narrow-band (high-Q) lithographic LC resonators. To prevent energy resolution degradation due to intermodulation line noise, the bias frequencies are distributed on a regular grid. The requirements on the accuracy of the LC resonance frequency are very high. The deviation of the resonance frequencies due to production tolerances is significant with respect to the bandwidth, and a controller is necessary to compensate for the LC series impedance. We present two such controllers: a simple orthogonal proportional-integrating (PI) controller and a more complex impedance estimator. Both controllers operate in baseband and try to make the TES current in-phase with the bias voltage, effectively operating as phase-locked loops (PLL). They allow off-LC-resonance operation of the TES pixels, while preserving TES thermal response and energy resolution. Extensive experimental results -- published in a companion paper recently -- with the proposed methods, show that these controllers allow the preservation of single pixel energy resolution in multiplexed operation.
We present X-ray absorption spectroscopy and resonant inelastic X-ray scattering (RIXS) measurements on the iron L-edge of 0.5 mM aqueous ferricyanide. These measurements demonstrate the ability of high-throughput transition-edge-sensor (TES) spectrometers to access the rich soft X-ray (100-2000eV) spectroscopy regime for dilute and radiation-sensitive samples. Our low-concentration data are in agreement with high-concentration measurements recorded by conventional grating-based spectrometers. These results show that soft X-ray RIXS spectroscopy acquired by high-throughput TES spectrometers can be used to study the local electronic structure of dilute metal-centered complexes relevant to biology, chemistry and catalysis. In particular, TES spectrometers have a unique ability to characterize frozen solutions of radiation- and temperature-sensitive samples.
We demonstrate the code-division multiplexed (CDM) readout of eight transition-edge sensor microcalorimeters. The energy resolution is 3.0 eV (full width at half-maximum) or better at 5.9 keV, with a best resolution of 2.3 eV and a mean of 2.6 eV over the seven modulated detectors. The flux-summing CDM system is described and compared with similar time-division multiplexed (TDM) readout. We show that the sqrt(Npixels) multiplexing disadvantage associated with TDM is not present in CDM. This demonstration establishes CDM as both a simple route to higher performance in existing TDM microcalorimetric experiments and a long-term approach to reaching higher multiplexing factors.
In this work, we present the first spectroscopic measurements of conversion electrons originating from the decay of metastable gaseous $^mathrm{83m}$Kr with the Karlsruhe Tritium Neutrino (KATRIN) experiment. The results obtained in this calibration measurement represent a major commissioning milestone for the upcoming direct neutrino mass measurement with KATRIN. The successful campaign demonstrates the functionalities of the full KATRIN beamline. The KATRIN main spectrometers excellent energy resolution of ~ 1 eV made it possible to determine the narrow K-32 and L$_3$-32 conversion electron line widths with an unprecedented precision of ~ 1 %.
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