This study deals with identifying some heavy metals (Pb,Zn,Ni) concentration in the recycledsewage in Latakia Countryside which is resulting from three treatment plants distributed over (Hebbeit, Al-Harah, MarjMoairban),2011.This research uses the Electro Thermal Atomization-Atomic Absorption Spectrometry (ETA-AAS) technique in determining of heavy metal elements mentioned above. This research shows a higher concentration of Zn-element (2.798 mg/L) in all treatment plants and in all seasons compared with the concentration of other elements, while Ni and Pb have recorded low concentrations (0.351, 0.243) mg/ℓ, respectively. The statistical study has demonstrated that there is a correlation varying from positive high to positive low, and sometimes to negative highs and lows, this gives clear indications for resources of pollution.