The Syrian natural zeolite from om'ozon area has been studied as adsorbent for Ni(II) ions from aqueous solution. The removal of Ni(II) ions under different conditions was studied adsorption of Ni(II) enhanced with an increase of initial concentration, temperature and PH .all experiments were carried out at contact time 6h. The amount of Ni(II) adsorption was increased from 16.36 mgNi/g for initial solution concentration of 100mg Ni/l to 71.33 mgNi/g (for C0=1000mgNi/L). The experimental data fitted well to Langmuir isotherm. The maximum capacity was qmax=142.85mgNi/g Adsorption amount at 298K varies from 16.36mgNi/g for initial solution concentration of 100mg Ni/l to 47.93mg Ni/g(for C0=400mgNi/L) and it increases at 333K to 16.65 mgNi/g and 51mgNi/g (for C0=100 and 400 mg Ni/L )respectively. The adsorption of Ni(II) ions was increased by increasing PH up to ~ 5 and then stabilized up to PH=6 and after that the precipitation process was accured.