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Register a new userLarge irreversibility field in nanoscale C-doped MgB2/Fe tape conductors
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We investigated the effect of nanoscale-C doping on the critical current density Jc and irreversibility field Birr of Fe-sheathed MgB2 tapes prepared by the in-situ powder-in-tube method. The tapes were heat treated at 600-950C for 1 h. Higher values of Jc and Birr were seen for 5 at.%C-doped MgB2 tapes at higher sintering temperatures, where substantial substitution of boron for carbon occurred. The C-doped samples sintered at 950C showed the highest Birr, for example, at 4.2 K, the Birr reached 22.9 T. In particular, at 20 K, Birr for the C-doped tape achieved 9 T, which is comparable to the upper critical field of the commercial NbTi at 4.2 K. This role of nano-sized C particles can be very beneficial in the fabrication of MgB2 tapes for magnetic resonance imaging applications at 20 K.
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Magnesium diboride (MgB2) powder was mechanically alloyed by high energy ball milling with C to a composition of Mg(B0.95C0.05)2 and then sintered at 1000 C in a hot isostatic press. Milling times varied from 1 minute to 3000 minutes. Full C incorporation required only 30-60 min of milling. Grain size of sintered samples decreased with increased milling time to less than 30 nm for 20-50 hrs of milling. Milling had a weak detrimental effect on connectivity. Strong irreversibility field (H*) increase (from 13.3 T to 17.2 T at 4.2 K) due to increased milling time was observed and correlated linearly with inverse grain size (1/d). As a result, high field Jc benefited greatly from lengthy powder milling. Jc(8 T, 4.2 K) peaked at > 80,000 A/cm2 with 1200 min of milling compared with only ~ 26,000 A/cm2 for 60 min of milling. This non-compositional performance increase is attributed to grain refinement of the unsintered powder by milling, and to the probable suppression of grain growth by milling-induced MgO nano-dispersions.
Fe-clad MgB2 long tapes have been fabricated using a powder-in-tube technique. An Mg + 2B mixture was used as the central conductor core and reacted in-situ to form MgB2. The tapes were sintered in pure Ar at 800 ^(o) C for 1 h at ambient pressure. SEM shows a highly dense core with a large grain size of 100 micron. The Fe clad tape shows a sharp transition with transition width of 0.2 K and Tc0 at 37.5 K. We have achieved the highest transport critical current reported so far at 1.6 times 10^(4) A/cm^2 for both 29.5 K in 1 Tesla and 33 K in null field. R-T and critical current were also measured for fields perpendicular and parallel to the tape plane. The iron cladding shielded on the core from the applied external field, with the shielding being less effective for the field in the tape plane. Fe cladding may be advantageous for some applications as it could reduce the effects of both the self-field and external fields.
We report the synthesis and variation of superconductivity parameters such as transition temperature Tc, upper critical field Hc, critical current density Jc, irreversibility field Hirr and flux pinning parameter (Fp) for the MgB2-xCx system with nano-Carbon doping up to x=0.20. Carbon substitutes successfully on boron site and results in significant enhancement of Hirr and Jc(H). Resistivity measurements reveal a continuous decrease in Tc under zero applied field, while the same improves remarkably at higher fields with an increase in nano-C content for MgB2-xCx system. The irreversibility field value (Hirr) is 7.6 & 6.6 Tesla at 5 and 10K respectively for the pristine sample, which is enhanced to 13.4 and 11.0 Tesla for x = .08 sample at same temperatures. Compared to undoped sample, critical current density (Jc) for the x=0.08 nano-Carbon doped sample is increased by a factor of 24 at 10K at 6 Tesla field.
MgB2 is a promising superconductor for important large-scale applications for both high field magnets and cryocooler-cooled magnet operated at temperatures around 20 K. In this work, by utilizing C60 as a viable alternative dopant, we demonstrate a simple and industrially scaleable rout that yields a 10-15-fold improvement in the in-high-field current densities of MgB2 tape conductors. For example, a Jc value higher than 4x10^4 A/cm^2 (4.2 K, 10 T), which exceeds that for NbTi superconductor, can be realized on the C60 doped MgB2 tapes. It is worth noting that this value is even higher than that fabricated using strict high energy ball milling technique under Ar atmosphere. At 20 K, Hirr was about 10 T for C60 doped MgB2 tapes. A large amount of nanometer-sized precipitates and grain boundaries were found in MgB2 matrix. The special physical and chemical characteristic of C60, in addition to its C containing intrinsic essence, is a key point in enhancing the superconducting performance of MgB2 tapes.
We consider the realistic case of a superconductor with a nonzero density of elastic scatterers, so that the normal state conductivity is finite. The quantum superconductor-metal (QSM) transition can then be tuned by varying either the attractive electron-electron interaction, the quenched disorder, or the applied magnetic field. We explore the consistency of the associated scaling relations, Tc ~ 1/lamda(0) ~ gap(0) ~ 1/gsi(0) ~ Hc2(0)^-0.5 and Tc(H) ~ 1/Lamda(0,H) ~ gap(0,h) ~ (Hc2(0)-H)^ 1/2, valid for all dimensions D > 2, with experimental data, in Al, C doped MgB2 and overdoped cuprates.
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