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The critical current density (Jc) of hot isostatic pressed (HIPed) MgB2 wires, measured by d.c. transport and magnetization, is compared with that of similar wires annealed at ambient pressure. The HIPed wires have a higher Jc than the annealed wires, especially at high temperatures and magnetic fields, and higher irreversibility field (Hirr). The HIPed wires are promising for applications, with Jc>106 A/cm2 at 5 K and zero field and >104 A/cm2 at 1.5 T and 26.5 K, and Hirr ~ 17 T at 4 K. The improvement is attributed to a high density of structural defects, which are the likely source of vortex pinning. These defects, observed by transmission electron microscopy, include small angle twisting, tilting, and bending boundaries, resulting in the formation of sub-grains within MgB2 crystallites.
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The microstructures of MgB2 wires prepared by the powder-in-tube technique and subsequent hot isostatic pressing were investigated using transmission electron microscopy. Large amount of crystalline defects including small angle twisting, tilting, and bending boundaries, in which high densities of dislocations reside, were found forming sub-grains within MgB2 grains. It is believed that these defects resulted from particle deformation during the hot isostatic pressing process and are effective flux pinning centers that contribute to the high critical current densities of the wires at high temperatures and at high fields.
We report dc transport and magnetization measurements of Jc in MgB2 wires fabricated by the powder-in-tube method, using commercial MgB2 powder with 5 %at Mg powder added as an additional source of magnesium, and stainless steel as sheath material. By appropriate heat treatments, we have been able to increase Jc by more than one order of magnitude from that of the as-drawn wire. We show that one beneficial effect of the annealing is the elimination of most of the micro-cracks, and we correlate the increase in Jc with the disappearance of the weak-link-type behavior.
We demonstrate that Fe sheathed LaO0.9F0.1FeAs wires with Ti as a buffer layer were successfully fabricated by the powder-in-tube (PIT) method. Comparing to the common two-step vacuum quartz tube synthesis method, the PIT method is more convenient and safe for synthesizing the novel iron-based layered superconductors. Structural analysis by mean of x-ray diffraction shows that the main phase of LaO0.9F0.1FeAs was obtained by this synthesis method. The transition temperature of the LaO0.9F0.1FeAs wire is around 25 K. The micrograph shows a homogeneous microstructure with a grain size of 1-3 micrometers. The results suggest that the PIT process is promising in preparing high-quality iron-based layered superconductor wires.
We report the fabrication of ErAl2 magnetocaloric wires by a powder-in-tube method (PIT) and the evaluation of magnetic entropy change through magnetization measurements. The magnetic entropy change of ErAl2 PIT wires exhibits similar behavior to the bulk counterpart, while its magnitude is reduced by the decrease in the volume fraction of ErAl2 due to the surrounding non-magnetic sheaths. We find that another effect reduces the magnetic entropy change of the ErAl2 PIT wires around the Curie temperature, and discuss its possible origin in terms of a correlation between magnetic properties of ErAl2 and mechanical properties of sheath material.
We present the fabrication and test results of Hot-Isostatic-Pressed (HIPed) Powder-in-Tube (PIT) MgB$_2$ coils. The coils properties were measured by transport and magnetization at different applied fields ($H$) and temperatures ($T$). The engineering critical current ($J_e$) value is the largest reported in PIT MgB$_2$ wires or tapes. At 25 K our champion 6-layer coil was able to generate a field of 1 T at self-field ($I_c >$ 220 A, $J_e sim 2.8 times 10^4$ A/cm$^2$). At 4 K this coil generated 1.6 T under an applied field of 1.25 T ($I_c sim350$ A, $J_e sim 4.5 times 10^4$ A/cm$^2$). These magnetic fields are high enough for a superconducting transformer or magnet applications such as MRI. A SiC doped MgB$_2$ single layer coil shows a promising improvement at high fields and exhibits $J_c > 10^4$ A/cm$^2$ at 7 T.
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