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Design and Commissioning of the PandaX-4T Cryogenic Distillation System for Krypton and Radon Removal

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 Added by Xiangyi Cui
 Publication date 2020
  fields Physics
and research's language is English




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An online cryogenic distillation system for the removal of krypton and radon from xenon was designed and constructed for PandaX-4T, a highly sensitive dark matter detection experiment. The krypton content in a commercial xenon product is expected to be reduced by 7 orders of magnitude with 99% xenon collection efficiency at a flow rate of 10 kg/h by design. The same system can reduce radon content in xenon by reversed operation, with an expected radon reduction factor of about 1.8 in PandaX-4T under a flow rate of 56.5 kg/h. The commissioning of this system was completed, with krypton and radon operations tested under respective working conditions. The krypton concentration of the product xenon was measured with an upper limit of 8.0 ppt.



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71 - Rui Yan , Zhou Wang , Xiangyi Cui 2021
An efficient cryogenic distillation system was designed and constructed for PandaX-4T dark matter detector based on the McCabe-Thiele (M-T) method and the conservation of mass and energy. This distillation system is designed to reduce the concentration of krypton in commercial xenon from 5X$10^{-7}$ mol/mol to $10^{-14}$ mol/mol with 99% xenon collection efficiency at a maximum flow rate of 10 kg/h. The offline distillation operation has been completed and 5.75 tons of ultra-high purity xenon was produced, which is used as the detection medium in PandaX-4T detector. The krypton concentration of the product xenon is measured with an upper limit of 8.0 ppt. The stability and purification performance of the cryogenic distillation system are studied by analyzing the experimental data, which is important for theoretical research and distillation operation optimization.
PandaX-4T is a dark matter direct detection experiment located in China jinping underground laboratory. The central apparatus is a dual-phase xenon detector containing 4 ton liquid xenon in the sensitive volume, with about 500 photomultipliers instrumented in the top and the bottom of the detector. In this paper we present a completely new system of readout electronics and data acquisition in the PandaX-4T experiment. Compared to the one used in the previous PandaX dark matter experiments, the new system features triggerless readout and higher bandwidth. With triggerless readout, dark matter searches are not affected by the efficiency loss of external triggers. The system records single photelectron signals of the dominant PMTs with an average efficiency of 96%, and achieves the bandwidth of more than 450 MB/s. The system has been used to successfully acquire data during the commissioning runs of PandaX-4T.
The XENON1T experiment aims for the direct detection of dark matter in a cryostat filled with 3.3 tons of liquid xenon. In order to achieve the desired sensitivity, the background induced by radioactive decays inside the detector has to be sufficiently low. One major contributor is the $beta$-emitter $^{85}$Kr which is an intrinsic contamination of the xenon. For the XENON1T experiment a concentration of natural krypton in xenon $rm{^{nat}}$Kr/Xe < 200 ppq (parts per quadrillion, 1 ppq = 10$^{-15}$ mol/mol) is required. In this work, the design of a novel cryogenic distillation column using the common McCabe-Thiele approach is described. The system demonstrated a krypton reduction factor of 6.4$cdot$10$^5$ with thermodynamic stability at process speeds above 3 kg/h. The resulting concentration of $rm{^{nat}}$Kr/Xe < 26 ppq is the lowest ever achieved, almost one order of magnitude below the requirements for XENON1T and even sufficient for future dark matter experiments using liquid xenon, such as XENONnT and DARWIN.
We have developed a low-energy electron recoil (ER) calibration method with $^{220}$Rn for the PandaX-II detector. $^{220}$Rn, emanated from natural thorium compounds, was fed into the detector through the xenon purification system. From 2017 to 2019, we performed three dedicated calibration campaigns with different radon sources. We studied the detector response to $alpha$, $beta$, and $gamma$ particles with focus on low energy ER events. During the runs in 2017 and 2018, the amount of radioactivity of $^{222}$Rn were on the order of 1% of that of $^{220}$Rn and thorium particulate contamination was negligible, especially in 2018. We also measured the background contribution from $^{214}$Pb for the first time in PandaX-II with the help from a $^{222}$Rn injection. Calibration strategy with $^{220}$Rn and $^{222}$Rn will be implemented in the upcoming PandaX-4T experiment and can be useful for other xenon-based detectors as well.
The KArlsruhe TRItium Neutrino (KATRIN) experiment, which aims to make a direct and model-independent determination of the absolute neutrino mass scale, is a complex experiment with many components. More than 15 years ago, we published a technical design report (TDR) [https://publikationen.bibliothek.kit.edu/270060419] to describe the hardware design and requirements to achieve our sensitivity goal of 0.2 eV at 90% C.L. on the neutrino mass. Since then there has been considerable progress, culminating in the publication of first neutrino mass results with the entire beamline operating [arXiv:1909.06048]. In this paper, we document the current state of all completed beamline components (as of the first neutrino mass measurement campaign), demonstrate our ability to reliably and stably control them over long times, and present details on their respective commissioning campaigns.
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