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Register a new userImpact of positive ion energy on carbon-surface production of negative ions in deuterium plasmas
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D. Kogut
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This work focuses on the production of negative-ions on graphite and diamond surfaces bombarded by positive ions in a low pressure (2 Pa) low power (20 W) capacitively coupled deuterium plasma. A sample is placed opposite a mass spectrometer and negatively biased so that surface produced negative ions can be self-extracted from the plasma and measured by the mass spectrometer. The ratio between negative-ion counts at mass spectrometer and positive ion current at sample surface defines a relative negative-ion yield. Changes in negative-ion production yields versus positive ion energy in the range 10-60 eV are analysed. While the negative-ion production yield is decreasing for diamond surfaces when increasing the positive ion impact energy, it is strongly increasing for graphite. This increase is attributed to the onset of the sputtering mechanisms between 20 and 40 eV which creates negative ions at rather low energy that are efficiently collected by the mass spectrometer. The same mechanism occurs for diamond but is mitigated by a strong decrease of the ionization probability due to defect creation and loss of diamond electronic properties.
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The production of negative ions is of significant interest for applications including mass spectrometry, materials surface processing, and neutral beam injection for magnetic confined fusion. Neutral beam injection sources maximise negative ion production through the use of surface production processes and low work function metals, which introduce complex engineering. Investigating materials and techniques to avoid the use of low work function metals is of interest to broaden the application of negative ion sources and simplify future devices. In this study, we use pulsed sample biasing to investigate the surface production of negative ions from nitrogen doped diamond. The use of a pulsed bias allows for the study of insulating samples in a preserved surface state at temperatures between 150$^{circ}$C and 700$^{circ}$C in a 2 Pa, 130 W, (n$_e$ $sim$ $10^9$ cm$^{-3}$, T$_e$ $sim$ 0.6 eV) inductively coupled deuterium plasma. The negative ion yield during the application of a pulsed negative bias is measured using a mass spectrometer and found to be approximately 20% higher for nitrogen doped diamond compared to non-doped diamond. It is also shown that the pulsed sample bias has a lower peak negative ion yield compared to a continuous sample bias, which suggests that the formation of an optimum ratio of defects on its surface can be favourable for negative ion production.
Coulomb implosion mechanism of the negatively charged ion acceleration in laser plasmas is proposed. When a cluster target is irradiated by an intense laser pulse and the Coulomb explosion of positively charged ions occurs, the negative ions are accelerated inward. The maximum energy of negative ions is several times lower than that of positive ions. The theoretical description and Particle-in-Cell simulation of the Coulomb implosion mechanism and the evidence of the negative ion acceleration in the experiments on the high intensity laser pulse interaction with the cluster targets are presented.
In this work negative-ion production on the surface of a sample negatively DC biased in a hydrogen plasma is studied. The negative ions created under the positive ion bombardment are accelerated towards the plasma, self-extracted and detected according to their energy and mass, by a mass spectrometer placed in front of the sample. The use of a pulsed bias allows applying a quasi-DC bias on insulating material during a short period of time and offers the possibility to extend the measurement method to nonconductive samples. The pulsed-bias tests were performed first with Highly Oriented Pyrolitic Graphite (HOPG), a conductive material, to demonstrate the feasibility of the method. By changing the pulsed-bias frequency it was possible to obtain HOPG material with different hydrogen surface coverages and hence different surface states leading to an increase of negative-ion production by up to 30-50% as compared to the continuous bias case. To establish a protocol for insulating materials, charge accumulation on the surface during the bias pulse and influence of the bias duration and frequency were explored using microcrystalline diamond (MCD) thin layers. By using a pulse short enough (10 $mu$s) at 1 kHz frequency, it has been possible to measure negative-ions on MCD sample at a quasi-constant surface bias of 130 V, with only 1 V variation during the measurement. Negative-ion surface production on MCD has been studied in pulsed mode with surface temperature from room temperature to 800{textdegree}C. It is shown that pulsing the bias and increasing the temperature allows limiting defect creation on MCD which is favorable for negative-ion production. Consequently, at 400{textdegree}C the yield on MCD in pulsed mode is one order of magnitude higher than the yield on HOPG in continuous mode at room temperature.
A model of the fluid nonlinear frequency shift of ion acoustic waves (IAWs) in multi-ion species plasmas is presented, which considers the effect of ion temperature. Because the thermal ion exists in plasmas in inertial confinement fusion (ICF) and also solar wind, which should be considered in nonlinear frequency shift of IAWs. However, the existing models [Berger et al., Physics of Plasmas 20, 032107 (2013); Q. S. Feng et al., Phys. Rev. E 94, 023205 (2016)] just consider the cold ion fluid models. This complete theory considering multi-ion species and thermal ions will calculate the frequency of the large amplitude nonlinear IAWs more accurately, especially the slow mode with high ion temperature, which will have wide application in space physics and inertial confinement fusion.
Weakly collisional Ar-O2 electronegative plasmas are investigated in a dc multidipole chamber. An electronegative core and an electropositive halo are observed. The density ratio of negative ions to electrons ({alpha}) in the nondrifting bulk is found to be 0.43. The profile of {alpha} is found using both the phase velocity of ion acoustic waves and the drift velocity of positive ions determined by laser induced fluorescence. The experiment shows that negative ions are in Boltzmann equilibrium with a temperature of 0.06 pm 0.02 eV. Double layers are not found separating the electronegative core and the electropositive halo.
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