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We have studied nucleation of magnetic domains and propagation of magnetic domain walls (DWs) induced by pulsed magnetic field in a ferromagnetic film with in-plane uniaxial anisotropy. Different from what have been seen up to now in out-of-plane anisotropy films, the nucleated domains have a rectangular shape in which a pair of the opposite sides are perfectly linear DWs, while the other pair present zigzags. This can be explained by magnetostatic optimization, knowing that the pulse field is applied parallel to the easy magnetization axis. The field induced propagation of these two DW types are very different. The linear ones follow a creep law identical to what is usually observed in out-of-plane films, when the velocity of zigzag DWs depends linearly on the applied field amplitude down to very low field. This most unusual feature can be explained by the shape of the DW, which makes it possible to go round the pinning defects. Thanks to that, it seems that propagation of zigzag walls agrees with the 1D model, and these results provide a first experimental evidence of the 1D model relevance in two dimensional ferromagnetic thin films. Lets note that it is the effective DW width parallel to DW propagation direction that matters in the 1D model formula, which is a relevant change when dealing with zigzag DWs.
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Chiral magnetic materials provide a number of challenging issues such as the highly efficient domain wall (DW) and skyrmion motions driven by electric current, as of the operation principles of emerging spintronic devices. The DWs in the chiral materials exhibit asymmetric DW speed variation under application of in plane magnetic field. Here, we show that such DW speed asymmetry causes the DW tilting during the motion along wire structure. It has been known that the DW tilting can be induced by the direct Zeeman interaction of the DW magnetization under application of in plane magnetic field. However, our experimental observations manifests that there exists another dominant process with the DW speed asymmetry caused by either the Dzyaloshinskii Moriya interaction (DMI) or the chirality dependent DW speed variation. A theoretical model based on the DW geometry reveals that the DW tilting is initiated by the DW pinning at wire edges and then, the direction of the DW tilting is determined by the DW speed asymmetry, as confirmed by a numerical simulation. The present observation reveals the decisive role of the DW pinning with the DW speed asymmetry, which determines the DW geometry and consequently, the dynamics.
The interfacial Dzyaloshinskii-Moriya interaction (DMI) is of great interest as it can stabilize chiral spin structures in thin films. Experiments verifying the orientation of the interfacial DMI vector remain rare, in part due to the difficulty of separating vector components of DMI. In this study, Fe/Ni bilayers and Co/Ni multilayers were deposited epitaxially onto Cu(001) and Pt(111) substrates, respectively. By tailoring the effective anisotropy, spin reorientation transitions (SRTs) are employed to probe the orientation of the DMI vector by measuring the spin structure of domain walls on both sides of the SRTs. The interfacial DMI is found to be sufficiently strong to stabilize chiral Neel walls in the out-of-plane magnetized regimes, while achiral Neel walls are observed in the in-plane magnetized regimes. These findings experimentally confirm that the out-of-plane component of the DMI vector is insignificant in these fcc(001) and fcc(111) oriented interfaces, even in the presence of atomic steps.
Using Lorentz transmission electron microscopy we investigate the behavior of domain walls pinned at non-topographic defects in Cr(3 nm)/Permalloy(10 nm)/Cr(5 nm) nanowires of width 500 nm. The pinning sites consist of linear defects where magnetic properties are modified by a Ga ion probe with diameter ~ 10 nm using a focused ion beam microscope. We study the detailed change of the modified region (which is on the scale of the focused ion spot) using electron energy loss spectroscopy and differential phase contrast imaging on an aberration (Cs) corrected scanning transmission electron microscope. The signal variation observed indicates that the region modified by the irradiation corresponds to ~ 40-50 nm despite the ion probe size of only 10 nm. Employing the Fresnel mode of Lorentz transmission electron microscopy, we show that it is possible to control the domain wall structure and its depinning strength not only via the irradiation dose but also the line orientation.
In chiral magnetic materials, numerous intriguing phenomena such as built in chiral magnetic domain walls (DWs) and skyrmions are generated by the Dzyaloshinskii Moriya interaction (DMI). The DMI also results in asymmetric DW speed under in plane magnetic field, which provides a useful scheme to measure the DMI strengths. However, recent findings of additional asymmetries such as chiral damping have disenabled unambiguous DMI determination and the underlying mechanism of overall asymmetries becomes under debate. By extracting the DMI-induced symmetric contribution, here we experimentally investigated the nature of the additional asymmetry. The results revealed that the additional asymmetry has a truly antisymmetric nature with the typical behavior governed by the DW chirality. In addition, the antisymmetric contribution changes the DW speed more than 100 times, which cannot be solely explained by the chiral damping scenario. By calibrating such antisymmetric contributions, experimental inaccuracies can be largely removed, enabling again the DMI measurement scheme.
Magnetic domain walls in thin films can be well analyzed using polarized neutron reflectometry. Well defined streaks in the off-specular spin-flip scattering maps are explained by neutron refraction at perpendicular N{e}el walls. The position of the streaks depends only on the magnetic induction within the domains, whereas the intensity of the off-specular magnetic scattering depends on the spin-flip probability at the domain walls and on the average size of the magnetic domains. This effect is fundamentally different and has to be clearly distinguished from diffuse scattering originating from the size distribution of magnetic domains. Polarized neutron reflectivity experiments were carried out using a $^3$He gas spin-filter with a analyzing power as high as 96% and a neutron transmission of approx 35%. Furthermore, the off-specular magnetic scattering was enhanced by using neutron resonance and neutron standing wave techniques.
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