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Tomographic Reconstruction of Triaxial Strain Fields from Bragg-Edge Neutron Imaging

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 Added by Johannes Hendriks
 Publication date 2019
and research's language is English




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This paper presents a proof-of-concept demonstration of triaxial strain tomography from Bragg-edge neutron imaging within a three-dimensional sample. Bragg-edge neutron transmission can provide high-resolution images of the average through thickness strain within a polycrystalline material. This poses an associated rich tomography problem which seeks to reconstruct the full triaxial strain field from these images. The presented demonstration is an important step towards solving this problem, and towards a technique capable of studying the residual strain and stress within engineering components. A Gaussian process based approach is used that ensures the reconstruction satisfies equilibrium and known boundary conditions. This approach is demonstrated experimentally on a non-trivial steel sample with use of the RADEN instrument at the Japan Proton Accelerator Research Complex. Validation of the reconstruction is provided by comparison with conventional strain scans from the KOWARI constant-wavelength strain diffractometer at the Australian Nuclear Science and Technology Organisation and simulations via finite element analysis.



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Energy resolved neutron transmission techniques can provide high-resolution images of strain within polycrystalline samples allowing the study of residual strain and stress in engineered components. Strain is estimated from such data by analysing features known as Bragg-edges for which several methods exist. It is important for these methods to provide both accurate estimates of strain and an accurate quantification the associated uncertainty. Our contribution is twofold. First, we present a numerical simulation analysis of these existing methods, which shows that the most accurate estimates of strain are provided by a method that provides inaccurate estimates of certainty. Second, a novel Bayesian non-parametric method for estimating strain from Bragg-edges is presented. The numerical simulation analysis indicates that this method provides both competitive estimates of strain and accurate quantification of certainty, two demonstrations on experimental data are then presented.
Several recent methods for tomographic reconstruction of stress and strain fields from Bragg-edge neutron strain images have been proposed in the literature. This paper presents an extension of a previously demonstrated approach based on Gaussian Process regression which enforces equilibrium in the method. This extension incorporates knowledge of boundary conditions, primarily boundary tractions, into the reconstruction process. This is shown to increase the rate of convergence and is more tolerant of systematic errors that may be present in experimental measurements. An exact expression for a central calculation in this method is also provided which avoids the need for the approximation scheme that was previously used. Convergence of this method for simulated data is compared to existing approaches and a reconstruction from experimental data is provided. Validation of the results to conventional constant wavelength strain measurements and comparison to prior methods shows a significant improvement.
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Nanoscale heterogeneity (including size, shape, strain, and defects) significantly impacts material properties and how they function. Bragg coherent x-ray imaging methods have emerged as a powerful tool to investigate, in three-dimensional detail, the local material response to external stimuli in reactive environments, thereby enabling explorations of the structure-defect-function relationship at the nanoscale. Although progress has been made in understanding this relationship, coherent imaging of extended samples is relatively slow (typically requiring many minutes) due to the experimental constraints required to solve the phase problem. Here, we develop Bragg coherent modulation imaging (BCMI), which uses a modulator to solve the phase problem thereby enabling fast, local imaging of an extended sample. Because a known modulator is essential to the technique, we first demonstrate experimentally that an unknown modulator structure can be recovered by using the exit wave diversity that exists in a standard Bragg coherent diffraction imaging (BCDI) experiment. We then show with simulations that a known modulator constraint is sufficient to solve the phase problem and enable a single view of an extended sample that is sensitive to defects and dislocations. Our results pave the way for BCMI investigations of strain and defect dynamics in complex extended crystals with temporal resolution limited by the exposure time of a single diffraction pattern.
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