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Register a new userMicrowave programmable response of Co-based microwire polymer composites through wire microstructure and arrangement optimization
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Traditional approaches to realize microwave tunability in microwire polymer composites which mainly rely on topological factors, magnetic field/stress stimuli, and hybridization prove to be burdensome and restricted to rather narrow band frequencies. This work presents a novel yet facile strategy based on a single component tunable medium to program the transmission response over wide frequency bands. To this end, we demonstrated that structural modification of one type of microwire through suitable current annealing and arrangement of the annealed wires in multiple combinations were sufficient to distinctly red-shift the transmission dip frequency of the composites. Such one wire control-strategy endorsed a programmable multivariable system grounded on the variations in both the overall array conductivity or effectiv area determined by the wires arrangement and the relaxation time dictated by the annealing degree of microwires. These results can be used to prescribe transmission frequency bands of desired features via diverse microwire arrays and microwave performance from a single component to a composite system design.
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The microwave properties of glass-fibers reinforced polymer composite embedded with an orthogonal array of Fe77Si10B10C3 microwires have been investigated. The composites containing orthogonal wire arrays display a remarkable transmission window in the frequency band of 1 to 6 GHz under zero external magnetic field indicating an intrinsic double-negative-index characteristic. The polymer matrices have proved to exert a synergistic effect on the microwave properties, which is responsible for the disappearance of the transmission windows when Ek is perpendicular to the glass fiber direction. The plasma frequency of the orthogonal microwire array composite is higher than that of the parallel microwire array with identical wire spacing; this could be attributed to the enhanced microwire-wave interaction induced by the axial electrical components on the additional layer of perpendicular wires. All these features make this new kind of orthogonal microwire composites promising for potential cloaking and sensing applications.
We aim at combining high coercivity magnetic nanowires in a polymer matrix in a view to fabricate rare--earth free bonded magnets. In particular, our aim is to fabricate anisotropic materials by aligning the wires in the polymer matrix. We have explored the different parameters of the fabrication process in order to produce a material with the best possible magnetic properties. We show that the choice of a proper solvent allows obtaining stable nanowire suspensions. The length and the type of the polymer chains play also an important role. Smaller chains ($M_w < 10000$) provide better magnetization results. The magnetic field applied during the casting of the material plays also a role and should be of the order of a fraction of a tesla. The local order of the nanowires in the matrix has been characterized by TEM and Small Angle Neutron Scattering. The correlation between the local order of the wires and the magnetic properties is discussed. Materials with coercivity $mu_0 H_c$ up to 0.70 $T$ at room temperature have been obtained.
A remarkably strong dependence of magnetoimpedance (MI) on tensile stress has been observed in the microwave frequency range for thin CoMnSiB glass-coated microwires exposed to a special thermal treatment. The MI ratio runs into more than 100% at 0.5-1.5 GHz when the tensile stress of 600 MPa is applied to the wire. It was demonstrated that a large MI change at such high frequencies is related predominantly with the dc magnetization orientation. A host of such microwires incorporated into a dielectric matrix may constitute a new sensing medium that is characterized by the stress-dependent effective permittivity. Such medium can be used for the microwave visualization of the stress distribution inside of a composite structure or on its surface.
We have investigated the microwave properties of epoxy-based composites containing melt-extracted Co69.25Fe4. 25B13.5-xSi13Nbx (x=0, 1, 3) microwires of various length annealed using a so-called combined current-modulation annealing (CCMA) technique. The observation of a double-peak feature in the permittivity spectra is believed due to the coexistence of the amorphous phase and a small amount of nanocrystallites on the wires with a high Nb content. CCMA was found to be favorable for a better-defined circular anisotropy of microwires and had suppressed the highfrequency peak due to residual stress relief for the composite with 25 mm long wires. Neither the shift of resonance peak nor the characteristic double peak feature was detected for composites containing as-cast 15 or 35 mm long microwires.
The microwave behavior of polymer metacomposites containing parallel Fe-based and continuous/short-cut Co-based microwire arrays has been investigated. A magnetic field-tunable metacomposite feature has been identified in the dense continuous hybrid composite confirmed by the transmission windows in the frequency band of 1 to 3.5 GHz. The complex magnetically tuned redshift-blueshift evolution of the transmission window is reasoned to result from the competition between the dynamic wire-wire interaction and the ferromagnetic resonance of Fe-based wires. Increasing Co-based inter-wire spacing to 10 mm in the continuous hybrid composites, a remarkable dual-band transmission window in the 1.5-3.5 GHz and 9-17 GHz is respectively induced by the ferromagnetic resonance of Fe-based wires and the magnetic resonance arising between Fe-Co wire couples. The hybridization of parallel Fe-based and short-cut Co-based wires in the polymer composite leads to a significant enhancement of the transmission window in the frequency band of 1 to 6 GHz due to the band-stop nature of Co-based wires. The advanced hybridized microwire metacomposites are arguably demonstrated to be particularly attractive for microwave cloaking and radio frequency barcoding applications.
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