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A compact imaging system with a CdTe double-sided strip detector for non-destructive analysis using negative muonic X-rays

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 Added by Miho Katsuragawa
 Publication date 2017
  fields Physics
and research's language is English




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A CdTe double-sided strip detector (CdTe-DSD) is an ideal device for imaging and spectroscopic measure- ments in the hard X-ray range above 10 keV. Recent development enables us to realize an imager with a detection area of ~10 cm${^2}$. An energy resolution of 1-2 keV (FWHM) and a position resolution of a few hundred {mu}m are available from the detector. This type of imager has been long awaited for non-destructive elemental analysis, especially by using negative muons, because energies of characteristic X-rays from muonic atoms are about 200 time higher than those from normal atoms. With the method that uses negative muons, hard X-ray information gives the spatial distribution of elements in samples at a certain depth defined by the initial momentum of the muon beam. In order to study three-dimensional imaging capability of the method, we have developed a compact imaging system based on CdTe-DSD and a {phi}3 mm pinhole collimator as the first prototype. We conducted experiments with samples which consist of layers of Al, BN and LiF irradiated by negative muon beams in MUSE/J-PARC and successfully reconstruct hard X-ray images of muonic X-rays from B, N and F at various depths.



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We have evaluated the performance of a fine pitch CdTe Double-sided Strip Detector (CdTe-DSD), which was originally developed for the focal plane detector of a hard X-ray telescope to observe the Sun. The detector has a thickness of 750 um and has 128 strip electrodes with a 60 um strip pitch orthogonally placed on both sides of the detector and covers an energy range 4 keV to 80 keV. The study of the depth of photon interaction and charge sharing effects are of importance in order to provide good spectroscopic and imaging performance. We study the tail structure observed in the spectra caused by charge trapping and develop a new method to reconstruct the spectra based on induced charge information from both anode and cathode strips. By applying this method, energy resolutions (FWHM) of 0.76 keV and 1.0 keV can be obtained at photon energies of 14 keV and 60 keV, respectively, if the energy difference between the anode and cathode is within 1 keV. Furthermore, the tail component at 60 keV is reduced, and the energy resolution of the 60 keV peak is improved from 2.4 keV to 1.5 keV (FWHM) if the energy difference is greater than 1 keV. In order to study the imaging performance, we constructed a simple imaging system using a 5 mm thick tungsten plate that has a pinhole with a diameter of 100 um. We utilize a Ba-133 radioisotope of 1 mm in diameter as a target source in combination with a 100 um slit made from 0.5 mm thickness tungsten. We imaged the Ba-133 source behind the 100 um slit using a 30 keV peak, with a 100 um pinhole placed at the center of the source-detector distance. By applying a charge sharing correction between strips, we have succeeded in obtaining a position resolution better than the strip pitch of 60 um.
The temperature of the working environment is a key factor in determining the properties of semiconductor detectors, and it affects the absolute accuracy and stability of the standard detector. In order to determine the temperature coefficient of CdTe detector used for X-rays detection, a precise temperature control system was designed. In this experiment, detectors and radiographic source were set inside the thermostat with temperature of 0-40 Celsius degree, so that the temperature can be regulated for the test of the temperature coefficient of CdTe detector. Studies had shown that, with the increase of the temperature, the energy resolution and detection efficiency of the CdTe detector would deteriorate, and under 10 Celsius degree the detectors have better performance with the 8 keV X-rays.
High-energy muons generated from cosmic-ray particle showers have been shown to exhibit properties ideal for imaging the interior of large structures. This paper explores the possibility of using a single portable muon detector in conjunction with image reconstruction methods used in nuclear medicine to reconstruct a 3D image of the interior of critical infrastructure such as the Zero Energy Deuterium (ZED-2) research reactor at Canadian Nuclear Laboratories Chalk River site. The ZED-2 reactor core and muon detector arrangement are modeled in GEANT4 and Monte Carlo measurements of the resultant muon throughput and angular distribution at several angles of rotation around the reactor are generated. Statistical analysis is then performed on these measurements based on the well-defined flux and angular distribution of muons expected near the surface of the earth. The results of this analysis are shown to produce reconstructed images of the spatial distribution of nuclear fuel within the core for multiple fuel configurations. This one-sided tomography concept is a possible candidate for examining the internal structure of larger critical facilities, for example the Fukushima Daiichi power plant where the integrity of the containment infrastructure and the location of the reactor fuel is unknown.
The performance of hybrid GaAs pixel detectors as X-ray imaging sensors were investigated at room temperature. These hybrids consist of 300 mu-m thick GaAs pixel detectors, flip-chip bonded to a CMOS Single Photon Counting Chip (PCC). This chip consists of a matrix of 64 x 64 identical square pixels (170 mu-m x 170 mu-m) and covers a total area of 1.2 cm**2. The electronics in each cell comprises a preamplifier, a discriminator with a 3-bit threshold adjust and a 15-bit counter. The detector is realized by an array of Schottky diodes processed on semi-insulating LEC-GaAs bulk material. An IV-charcteristic and a detector bias voltage scan showed that the detector can be operated with voltages around 200 V. Images of various objects were taken by using a standard X-ray tube for dental diagnostics. The signal to noise ratio (SNR) was also determined. The applications of these imaging systems range from medical applications like digital mammography or dental X-ray diagnostics to non destructive material testing (NDT). Because of the separation of detector and readout chip, different materials can be investigated and compared.
The imaging and spectral performance of CdTe double-sided strip detectors (CdTe-DSDs) was evaluated for the ASTRO-H mission. The charcterized CdTe-DSDs have a strip pitch of 0.25 mm, an imaging area of 3.2 cm$times$3.2 cm and a thickness of 0.75 mm. The detector was successfully operated at a temperature of $-20^circ$C and with an applied bias voltage of 250 V. By using two-strip events as well as one-strip events for the event reconstruction, a good energy resolution of 2.0 keV at 59.5 keV and a sub-strip spatial resolution was achieved. The hard X-ray and gamma-ray response of CdTe-DSDs is complex due to the properties of CdTe and the small pixel effect. Therefore, one of the issues to investigate is the response of the CdTe-DSD. In order to investigate the spatial dependence of the detector response, we performed fine beam scan experiments at SPring-8, a synchrotron radiation facility. From these experiments, the depth structure of the electric field was determined as well as properties of carriers in the detector and successfully reproduced the experimental data with simulated spectra.
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