Investigating the role of causal order in quantum mechanics has recently revealed that the causal distribution of events may not be a-priori well-defined in quantum theory. While this has triggered a growing interest on the theoretical side, creating processes without a causal order is an experimental task. Here we report the first decisive demonstration of a process with an indefinite causal order. To do this, we quantify how incompatible our set-up is with a definite causal order by measuring a causal witness. This mathematical object incorporates a series of measurements which are designed to yield a certain outcome only if the process under examination is not consistent with any well-defined causal order. In our experiment we perform a measurement in a superposition of causal orders - without destroying the coherence - to acquire information both inside and outside of a causally non-ordered process. Using this information, we experimentally determine a causal witness, demonstrating by almost seven standard deviations that the experimentally implemented process does not have a definite causal order.
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