Sign reversal of the Hall resistance in the mixed-state of La$_{1.89}$ Ce$_{0.11}$CuO$_{4}$ and La$_{1.89}$Ce$_{0.11}$(Cu$_{0.99}$Co$_{0.01}$)O$_{4} $ thin films
The transport properties of La$_{1.89}$Ce$_{0.11}$CuO$_{4}$(LCCO) and La$_{1.89}$Ce$_{0.11}$(Cu$_{0.99}$Co$_{0.01}$)O$_{4}$ (LCCO:Co) superconducting thin films are investigated. When the external field $bf H$ is applied along the crystallographic c-axis, a double sign reversal of the Hall voltage in the mixed state of LCCO:Co thin films is observed whereas a single sign reversal is detected in LCCO. A double sign reversal of the Hall signal in LCCO can be recovered if the magnetic field is tilted away from the plane of the film. We find that the transition from one to two of the Hall sign reversal coincides with the change in the pinning from strong to weak. This temperature/field induced transition is caused either by the magnetic impurities in LCCO:Co or by the coupling between the pancake vortices and the in-plane Josephson vortices in LCCO. These results are in agreement with early theoretical and numerical predictions.
We report a study of the microwave conductivity of electron-doped Pr$_{1.85}$Ce$_{0.15}$CuO$_{4-delta}$ superconducting thin films using a cavity perturbation technique. The relative frequency shifts obtained for the samples placed at a maximum electric field location in the cavity are treated using the high conductivity limit presented recently by Peligrad $textit{et}$ $textit{al.}$ Using two resonance modes, TE$_{102}$ (16.5 GHz) and TE$_{101}$ (13 GHz) of the same cavity, only one adjustable parameter $Gamma$ is needed to link the frequency shifts of an empty cavity to the ones of a cavity loaded with a perfect conductor. Moreover, by studying different sample configurations, we can relate the substrate effects on the frequency shifts to a scaling factor. These procedures allow us to extract the temperature dependence of the complex penetration depth and the complex microwave conductivity of two films with different quality. Our data confirm that all the physical properties of the superconducting state are consistent with an order parameter with lines of nodes. Moreover, we demonstrate the high sensitivity of these properties on the quality of the films.
We report $^{139}$La and $^{63}$Cu NMR investigation of the successive charge order, spin order, and superconducting transitions in super-oxygenated La$_2$CuO$_{4+y}$ single crystal with stage-4 excess oxygen order at $T_{stage}simeq 290$ K. We show that the stage-4 order induces tilting of CuO$_6$ octahedra below $T_{stage}$, which in turn causes $^{139}$La NMR line broadening. The structural distortion continues to develop far below $T_{stage}$, and completes at $T_{charge}simeq 60$ K, where charge order sets in. This sequence is reminiscent of the the charge order transition in Nd co-doped La$_{1.88}$Sr$_{0.12}$CuO$_4$ that sets in once the low temperature tetragonal (LTT) phase is established. We also show that the paramagnetic $^{63}$Cu NMR signals are progressively wiped out below $T_{charge}$ due to enhanced low frequency spin fluctuations, but the residual $^{63}$Cu NMR signals continue to exhibit the characteristics expected for optimally doped superconducting CuO$_2$ planes. This indicates that charge order in La$_2$CuO$_{4+y}$ does not take place uniformly in space. Low frequency Cu spin fluctuations as probed by $^{139}$La nuclear spin-lattice relaxation rate are mildly glassy, and do not exhibit critical divergence at $T_{spin}$($simeq T_{c}$)=42 K. These findings, including the spatially inhomogeneous nature of the charge ordered state, are qualitatively similar to the case of La$_{1.885}$Sr$_{0.115}$CuO$_4$ [T. Imai et al., Phys. Rev. B 96 (2017) 224508, and A. Arsenault et al., Phys. Rev. B 97 (2018) 064511], but both charge and spin order take place more sharply in the present case.
The presence of a small concentration of in-plane Fe dopants in La$_{1.87}$Sr$_{0.13}$Cu$_{0.99}$Fe$_{0.01}$O$_4$ is known to enhance stripe-like spin and charge density wave (SDW and CDW) order, and suppress the superconducting $T_c$. Here, we show that it also induces highly two-dimensional (2D) superconducting correlations that have been argued to be signatures of a new form of superconducting order, so-called pair-density-wave (PDW) order. In addition, using the resonant soft x-ray scattering, we find that the 2D superconducting fluctuation is strongly associated with the CDW stripe. In particular, the PDW signature first appears when the correlation length of the CDW stripe grows over eight times the lattice unit ($sim$ 8$a$). These results provide critical conditions for the formation of PDW order.
For electron-doped cuprates, the strong suppression of antiferromagnetic spin correlation by efficient reduction annealing by the protect-annealing method leads to superconductivity not only with lower Ce concentrations but also with higher transition temperatures. To reveal the nature of this superconducting state, we have performed angle-resolved photoemission spectroscopy measurements of protect-annealed electron-doped superconductors Pr$_{1.3-x}$La$_{0.7}$Ce$_{x}$CuO$_{4}$ and directly investigated the superconducting gap. The gap was found to be consistent with $d$-wave symmetry, suggesting that strong electron correlation persists and hence antiferromagnetic spin fluctuations remain a candidate that mediates Copper pairing in the protect-annealed electron-doped cuprates.
We present results of magnetic neutron diffraction experiments on the co-doped super-oxygenated La(2-x)Sr(x)CuO(4+y) (LSCO+O) system with x=0.09. The spin-density wave has been studied and we find long-range incommensurate antiferromagnetic order below T_N coinciding with the superconducting ordering temperature T_c=40 K. The incommensurability value is consistent with a hole-doping of n_h~1/8, but in contrast to non-superoxygenated La(2-x)Sr(x)CuO(4) with hole-doping close to n_h ~ 1/8 the magnetic order parameter is not field-dependent. We attribute this to the magnetic order being fully developed in LSCO+O as in the other striped lanthanum-cuprate systems.
K. Jin
,B. X. Wu
,B. Y. Zhu
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(2011)
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"Sign reversal of the Hall resistance in the mixed-state of La$_{1.89}$ Ce$_{0.11}$CuO$_{4}$ and La$_{1.89}$Ce$_{0.11}$(Cu$_{0.99}$Co$_{0.01}$)O$_{4} $ thin films"
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Kui Jin
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