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Register a new userUnambiguous determination of structure parameters for soft matter samples made possible with polarization analysis on JCNS SANS using a 3He spin filter
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Incoherent background can create an intrinsic problem for standard small angle neutron scattering measurements. Biological samples contain hydrogen which is a strong incoherent scatterer thus creating an intrinsic source of background that makes determination of the coherent scattering parameters difficult in special situations. This can especially be true for the Q-range from around 0.1-0.5 AA^-1 where improper knowledge of the background level can lead to ambiguity in determination of the samples structure parameters. Polarization analysis is a way of removing this ambiguity by allowing one to distinguish the coherent from incoherent scattering, even when the coherent scattering is only a small fraction of the total scattered intensity. ^3He spin filters are ideal for accomplishing this task because they permit the analysis of large area and large divergence scattered neutron beams without adding to detector background or changing the prorogation of the scattered neutron beam. This rapid note describes the application of ^3He neutron spin filters, polarized using the spin-exchange optical pumping method, for polarization analysis on a protein sample to unambiguously extract the coherent scattered intensity.
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Accurately measuring the neutron beam polarization of a high flux, large area neutron beam is necessary for many neutron physics experiments. The Fundamental Neutron Physics Beamline (FnPB) at the Spallation Neutron Source (SNS) is a pulsed neutron beam that was polarized with a supermirror polarizer for the NPDGamma experiment. The polarized neutron beam had a flux of $sim10^9$ neutrons per second per cm$^2$ and a cross sectional area of 10$times$12~cm$^2$. The polarization of this neutron beam and the efficiency of a RF neutron spin rotator installed downstream on this beam were measured by neutron transmission through a polarized $^{3}$He neutron spin-filter. The pulsed nature of the SNS enabled us to employ an absolute measurement technique for both quantities which does not depend on accurate knowledge of the phase space of the neutron beam or the $^{3}$He polarization in the spin filter and is therefore of interest for any experiments on slow neutron beams from pulsed neutron sources which require knowledge of the absolute value of the neutron polarization. The polarization and spin-reversal efficiency measured in this work were done for the NPDGamma experiment, which measures the parity violating $gamma$-ray angular distribution asymmetry with respect to the neutron spin direction in the capture of polarized neutrons on protons. The experimental technique, results, systematic effects, and applications to neutron capture targets are discussed.
Exploiting small angle X-ray and neutron scattering (SAXS/SANS) on the same sample volume at the same time provides complementary nanoscale structural information at two different contrast situations. Compared with an independent experimental approach, the truly combined SAXS/SANS experimental approach ensures the exactness of the probed samples particularly for in-situ studies. Here, we introduce an advanced portable SAXS system that is dimensionally suitable for installation at D22 zone of ILL. The SAXS apparatus is based on a RIGAKU copper/molybdenum switchable microfocus rotating anode X-ray generator and a DECTRIS detector with a changeable sample-to-detector distance of up to 1.6 m in a vacuum chamber. A science case has been presented to demonstrate the uniqueness of the newly established method at ILL. Temporal structural rearrangements of both, organic stabilizing agents and organically capped gold colloidal particles during gold nanoparticle growth are simultaneously probed, enabling immediate correlated structural information. The newly established nano-analytical method at ILL will open the way for real time investigations of a wide range of innovative nanomaterials and will enable comprehensive in-situ studies on biological systems. A potential development of a fully-automated SAXS/SANS system with a common control environment and additional sample environments, permitting a continual and efficient operation of the system at the hands of ILL users, has also been introduced.
The neutron polarization of the NG-C beamline at the NIST Center for Neutron Research was measured as part of the aCORN neutron beta decay experiment. Neutron transmission through a polarized 3He spin filter cell was recorded while adiabatic fast passage (AFP) nuclear magnetic resonance (NMR) reversed the polarization direction of the 3He in an eight-step sequence to account for drifts. The dependence of the neutron transmission on the spin filter direction was used to calculate the neutron polarization. The time dependent transmission was fit to a model which included the neutron spectrum, and 3He polarization losses from spin relaxation and AFP-NMR. The polarization of the NG-C beamline was found to be ${mid}P_mathrm{n}{mid} leq 4times 10^{-4}$ with 90 % confidence.
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