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Register a new userRadiation hardness qualification of PbWO4 scintillation crystals for the CMS Electromagnetic Calorimeter
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Ensuring the radiation hardness of PbWO4 crystals was one of the main priorities during the construction of the electromagnetic calorimeter of the CMS experiment at CERN. The production on an industrial scale of radiation hard crystals and their certification over a period of several years represented a difficult challenge both for CMS and for the crystal suppliers. The present article reviews the related scientific and technological problems encountered.
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Kinetics of radiation damage of the PWO crystals under irradiation and recovery were studied. Crystals were irradiated with dose corresponding to average one expected in the electromagnetic calorimeter (working dose irradiation). Radiation damage and recovery were monitored through measurements of PWO optical transmission. An approach is proposed which allows evaluating the influence of the PWO crystals properties on the statistical term in the energy resolution of the electromagnetic calorimeter. The analysis also gives important information about the nature of the radiation damage mechanism in scintillation crystals. The method was used during development of technology of the mass production of radiation hard crystals and during development of methods for crystals certification
Pixel detectors are used in the innermost part of the multi purpose experiments at LHC and are therefore exposed to the highest fluences of ionising radiation, which in this part of the detectors consists mainly of charged pions. The radiation hardness of all detector components has thoroughly been tested up to the fluences expected at the LHC. In case of an LHC upgrade, the fluence will be much higher and it is not yet clear how long the present pixel modules will stay operative in such a harsh environment. The aim of this study was to establish such a limit as a benchmark for other possible detector concepts considered for the upgrade. As the sensors and the readout chip are the parts most sensitive to radiation damage, samples consisting of a small pixel sensor bump-bonded to a CMS-readout chip (PSI46V2.1) have been irradiated with positive 200 MeV pions at PSI up to 6E14 Neq and with 21 GeV protons at CERN up to 5E15 Neq. After irradiation the response of the system to beta particles from a Sr-90 source was measured to characterise the charge collection efficiency of the sensor. Radiation induced changes in the readout chip were also measured. The results show that the present pixel modules can be expected to be still operational after a fluence of 2.8E15 Neq. Samples irradiated up to 5E15 Neq still see the beta particles. However, further tests are needed to confirm whether a stable operation with high particle detection efficiency is possible after such a high fluence.
This paper is devoted to the study of a degradation of CsI(Tl)crystals scintillation characteristics under irradiation with gamma-quanta at the uniformly distributed absorbed dose up to 3700 rad. The sample set consisted of 25 crystals of 30 cm long having a truncated pyramid shape and 30 rectangular crystals of the same length. A large difference in the light output deterioration caused by the radiation was observed for the samples of the same shape. A substantial dependence of the average light output loss from the sample shape is seen as well. On the other hand, the crystals from the same ingot behave very similarly under irradiation.
We employed two independent methods to study possible damage to the scintillation mechanism in lead tungstate crystals due to irradiation by a 34 GeV pion beam. First, 10 crystals were irradiated simultaneously over 30 hours by a narrow beam, so that only a small region of each crystal was affected. We studied the effect of the irradiation on the light output non-uniformity. If a localized degradation was observed, it would indicate damage to the scintillation mechanism. Secondly, we detected light output using two phototubes attached to sides of a crystal. Since these phototubes detect scintillation light only from a small localized region, the effect of transmission loss should be minimal. We did not see any statistically significant evidence for scintillation mechanism damage with either method. The effect is consistent with zero, and the upper limit is 0.5% at 95% C.L.
Lead fluoride ($PbF_{2}$) crystals represent an excellent and relatively innovative choice for high resolution electromagnetic calorimeters with high granularity and fast timing. During the R&D stages of the Crilin calorimeter, three pbfd crystals sized $5times 5 times 40 $ mm$^3$ were irradiated with $^{60}$Co photons up to $sim 4$ Mrad and with 14 MeV neutrons up to a $10^{13}$ n/cm$^2$ total fluence. Their loss in transmittance was evaluated at different steps of the photon and neutron irradiation campaign, and two optical absorption bands associated with the formation of colour centres were observed at $sim 270$ nm and $sim 400$ nm. Natural and thermal annealing in the dark, along with optical bleaching with 400 nm light, were performed on the irradiated specimens resulting in a partial recovery of their original optical characteristics.
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