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تسجيل مستخدم جديدFermilab experience of post-annealing losses in SRF niobium cavities due to furnace contamination and the ways to its mitigation: a pathway to processing simplification and quality factor improvement
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We investigate the effect of high temperature treatments followed by only high-pressure water rinse (HPR) of superconducting radio frequency (SRF) niobium cavities. The objective is to provide a cost effective alternative to the typical cavity processing sequence, by eliminating the material removal step post furnace treatment while preserving or improving the RF performance. The studies have been conducted in the temperature range 800-1000C for different conditions of the starting substrate: large grain and fine grain, electro-polished (EP) and centrifugal barrel polished (CBP) to mirror finish. An interesting effect of the grain size on the performances is found. Cavity results and samples characterization show that furnace contaminants cause poor cavity performance, and a practical solution is found to prevent surface contamination. Extraordinary values of residual resistances ~ 1 nOhm and below are then consistently achieved for the contamination-free cavities. These results lead to a more cost-effective processing and improved RF performance, and, in conjunction with CBP, open a potential pathway to acid-free processing.
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We report a surface treatment that systematically improves the quality factor of niobium radio frequency cavities beyond the expected limit for niobium. A combination of annealing in a partial pressure of nitrogen or argon gas and subsequent electrop
olishing of the niobium cavity surface leads to unprecedented low values of the microwave surface resistance, and an improvement in the efficiency of the accelerating structures up to a factor of 3, reducing the cryogenic load of superconducting cavities for both pulsed and continuous duty cycles. The field dependence of the surface resistance is reversed compared to standardly treated niobium.
In this study, we present new insights on the origin of the high-field Q-slope in superconducting radio-frequency cavities. Consequent hydrofluoric acid rinses are used to probe the radio-frequency performance as a function of the material removal of
two superconducting bulk niobium cavities prepared with low temperature nitrogen infusion. The study reveals that nitrogen infusion affects only the first few tens of nanometers below the native oxide layer. The typical high-field Q-slope behavior of electropolished cavities is indeed completely recovered after a dozen hydrofluoric acid rinses. The reappearance of the high-field Q-slope as a function of material removal was modeled by means of Londons local description of screening currents in the superconductor, returning good fitting of the experimental data and suggesting that interstitial impurities layers with diffusion length of the order to tens of nanometers can mitigate high-field Q-slope.
Ambient magnetic field, if trapped in the penetration depth, leads to the residual resistance and therefore sets the limit for the achievable quality factors in superconducting niobium resonators for particle accelerators. Here we show that a complet
e expulsion of the magnetic flux can be performed and leads to: 1) record quality factors $Q > 2times10^{11}$ up to accelerating gradient of 22 MV/m; 2) $Qsim3times10^{10}$ at 2 K and 16 MV/m in up to 190 mG magnetic fields. This is achieved by large thermal gradients at the normal/superconducting phase front during the cooldown. Our findings open up a way to ultra-high quality factors at low temperatures and show an alternative to the sophisticated magnetic shielding implemented in modern superconducting accelerators.
Cool-down dynamics of superconducting accelerating cavities became particularly important for obtaining very high quality factors in SRF cavities. Previous studies proved that when cavity is cooled fast, the quality factor is higher than when cavity
is cooled slowly. This has been discovered to derive from the fact that a fast cool-down allows better magnetic field expulsion during the superconducting transition. In this paper we describe the first experiment where the temperature all around the cavity was mapped during the cavity cool-down through transition temperature, proving the existence of two different transition dynamics: a sharp superconducting-normal conducting transition during fast cool-down which favors flux expulsion and nucleation phase transition during slow cool-down, which leads to full flux trapping.
Buffered Chemical Polishing (BCP) was the most conventional polishing method for superconducting radio frequency (SRF) Niobium (Nb) cavity surface preparation before the discovery of Electropolishing (EP), which is superior to BCP in high gradient pe
rformance. The High Field Q-slope (HFQS) is perfectly eliminated by taking the low temperature bake (LTB) post EP, which guarantees high gradient performance in EPed cavities. The mechanism of the HFQS is well understood for EPed cavities. On the other hand, there is no common consensus on the HFQS with BCP, since even BCP with LTB does not always resolve the HFQS. BCP is much easier to apply and still an important preparation technology for very complicated SRF structures like low beta cavities. Therefore, overcoming the issue of HFQS with BCP is highly beneficial to the SRF community. This paper mines a large number of available data sets on BCPed cavity performance with fine grain, large grain, and even single crystal niobium materials under different experimental settings. We found that all existing explanations for HFQS with BCP are inconsistent with some experimental results, and propounded nitrogen contamination as a new model. We checked that nitrogen contamination agrees with all existing data and nicely explains unresolved phenomena. Combining these evidence, we deduce that nitrogen contamination is the cause of HFQS in BCP.
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